Benzoic acid, 4-hydroxy-, 6-hydroxyhexyl ester

Base Information

• Chemical Name: Benzoic acid, 4-hydroxy-, 6-hydroxyhexyl ester
• CAS No.: 62702-43-6
• Molecular Formula: C13H18O4
• Molecular Weight: 238.28000
• Mol file: 62702-43-6.mol

Synonyms:Benzoic acid,4-hydroxy-,6-hydroxyhexyl ester;4-Hydroxy-benzoesaeure-(6-hydroxy-hexylester);4-hydroxy-benzoic acid-(6-hydroxy-hexyl ester);

Chemical Property of Benzoic acid, 4-hydroxy-, 6-hydroxyhexyl ester

Chemical Property:

• PSA: 66.76000
• LogP: 2.10170

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Benzoic acid, 4-hydroxy-, 6-hydroxyhexyl ester

There total 4 articles about Benzoic acid, 4-hydroxy-, 6-hydroxyhexyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

6-chloro-1-hexanol (2009-83-8) + 4-hydroxy-benzoic acid (99-96-7) → 6-Hydroxyhexyl 4-hydroxybenzoate (62702-43-6)

Guidance literature:

With potassium hydrogencarbonate; In dimethyl sulfoxide; at 80 ℃; for 5h;

DOI:10.1080/10587259408037766

Reference yield:

4-ethoxycarbonyloxy-benzoic acid-(6-hydroxy-hexyl ester) (250378-28-0) → 6-Hydroxyhexyl 4-hydroxybenzoate (62702-43-6)

Guidance literature:

With sodium hydroxide;

Reference yield:

4-Ethoxycarbonyloxybenzoic acid (15552-32-6) → 6-Hydroxyhexyl 4-hydroxybenzoate (62702-43-6)

Guidance literature:

Multi-step reaction with 3 steps

1: SOCl₂

2: 1,2-dichloro-ethane

3: aq.-ethanolic NaOH

With sodium hydroxide; thionyl chloride; 1,2-dichloro-ethane;

upstream raw materials:

4-ethoxycarbonyloxy-benzoic acid-(6-hydroxy-hexyl ester)

6-chloro-1-hexanol

4-hydroxy-benzoic acid

4-Ethoxycarbonyloxybenzoic acid