Diethyl methyl[4-(2-methylpropyl)phenyl]propanedioate

Base Information

Chemical Name:Diethyl methyl[4-(2-methylpropyl)phenyl]propanedioate
CAS No.:62707-18-0
Molecular Formula:C18H26O4
Molecular Weight:306.402
Hs Code.:
DSSTox Substance ID:DTXSID50503556
Wikidata:Q82357480

Synonyms:62707-18-0;Diethyl methyl[4-(2-methylpropyl)phenyl]propanedioate;DTXSID50503556

Suppliers and Price of Diethyl methyl[4-(2-methylpropyl)phenyl]propanedioate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Diethyl methyl[4-(2-methylpropyl)phenyl]propanedioate

Chemical Property:

XLogP3:4.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:9
Exact Mass:306.18310931
Heavy Atom Count:22
Complexity:349

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCOC(=O)C(C)(C1=CC=C(C=C1)CC(C)C)C(=O)OCC

Technology Process of Diethyl methyl[4-(2-methylpropyl)phenyl]propanedioate

There total 7 articles about Diethyl methyl[4-(2-methylpropyl)phenyl]propanedioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 74610-74-5
p-isobutylphenyllead triacetate

: 609-08-5
Diethyl methylmalonate

: 62707-18-0
diethyl 2-(p-isobutylphenyl)-2-methylpropanedioate

Guidance literature:: In tetrahydrofuran; pyridine; for 1h; Ambient temperature; The sodium salt of the β-dicarbonyl compound was generated at first.;
DOI:10.1016/S0040-4039(00)77752-5

Reference yield: 74.0%

: 62116-54-5
sodium diethyl methylmalonate

: 74610-74-5
p-isobutylphenyllead triacetate

: 62707-18-0
diethyl 2-(p-isobutylphenyl)-2-methylpropanedioate

Guidance literature:: With pyridine; In tetrahydrofuran; for 1h; Ambient temperature;

Reference yield:

: 538-93-2
1-phenyl-2-methylpropane

: 62707-18-0
diethyl 2-(p-isobutylphenyl)-2-methylpropanedioate

Guidance literature:: Multi-step reaction with 3 steps

1: 94 percent / SnCl₄ / CH₂Cl₂ / 1.) 0 deg C, 10 min, 2.) 20 deg C, 3 h

2: 80 percent / Et₃N, 4-(dimethylamino)pyridine / CH₂Cl₂ / 48 h / 20 °C

3: 1.) sodium α-(dimethylamino)naphthalenide / 1.) benzene, HMPA, 30 s, 2.) 30 min

With dmap; sodium α-(dimethylamino)naphthalenide; tin(IV) chloride; triethylamine; In dichloromethane;
DOI:10.1021/jo00145a017