2-Chloro-1,1,3,3-tetramethyl-2-nitrosocyclohexane

Base Information

Chemical Name:2-Chloro-1,1,3,3-tetramethyl-2-nitrosocyclohexane
CAS No.:62735-89-1
Molecular Formula:C10H18ClNO
Molecular Weight:203.712
Hs Code.:
DSSTox Substance ID:DTXSID60518035

Synonyms:2-Chloro-1,1,3,3-tetramethyl-2-nitrosocyclohexane;62735-89-1;DTXSID60518035

Suppliers and Price of 2-Chloro-1,1,3,3-tetramethyl-2-nitrosocyclohexane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-Chloro-1,1,3,3-tetramethyl-2-nitrosocyclohexane

Chemical Property:

XLogP3:3.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:0
Exact Mass:203.1076919
Heavy Atom Count:13
Complexity:207

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1(CCCC(C1(N=O)Cl)(C)C)C

Technology Process of 2-Chloro-1,1,3,3-tetramethyl-2-nitrosocyclohexane

There total 3 articles about 2-Chloro-1,1,3,3-tetramethyl-2-nitrosocyclohexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 7007-40-1
2,2,6,6-Tetramethylcyclohexanone oxime

: 2899-02-7,99515-28-3
N,N'-dichlorobis(2,4,6-trichlorodiphenyl)urea

: 62735-89-1
α-chloro-nitroso-2,2,6,6-tetramethylcyclohexane

: 20632-35-3
bis(2,4,6-trichlorodiphenyl)urea

Guidance literature:: In acetonitrile; at 20 ℃; for 0.5h;
DOI:10.1016/j.tetlet.2006.12.001

Reference yield: 88.0%

: 7007-40-1
2,2,6,6-Tetramethylcyclohexanone oxime

: 62735-89-1
α-chloro-nitroso-2,2,6,6-tetramethylcyclohexane

Guidance literature:: With tert-butylhypochlorite; In dichloromethane; tert-butyl alcohol; at 0 ℃; for 1.5h;
DOI:10.1055/s-2005-918429

Reference yield:

: 1195-93-3
2,2,6,6-tetramethylcyclohexanone

: 62735-89-1
α-chloro-nitroso-2,2,6,6-tetramethylcyclohexane

Guidance literature:: Multi-step reaction with 2 steps

1: 73 percent / NH₂OH*HCl; NaOAc / methanol / 72 h / Heating

2: 88 percent / t-BuOCl / CH₂Cl₂; 2-methyl-propan-2-ol / 1.5 h / 0 °C

With tert-butylhypochlorite; hydroxylamine hydrochloride; sodium acetate; In methanol; dichloromethane; tert-butyl alcohol;
DOI:10.1055/s-2005-918429