2-Propenoic acid, 3-[5-(4-nitrophenyl)-2-furanyl]-, (E)-

Base Information

Chemical Name:2-Propenoic acid, 3-[5-(4-nitrophenyl)-2-furanyl]-, (E)-
CAS No.:62806-39-7
Molecular Formula:C13H9NO5
Molecular Weight:259.218
Hs Code.:
DSSTox Substance ID:DTXSID80356916

Synonyms:2-Propenoic acid, 3-[5-(4-nitrophenyl)-2-furanyl]-, (E)-;CBDivE_012196;3-[5-(4-nitrophenyl)furan-2-yl]prop-2-enoic acid;DTXSID80356916

Suppliers and Price of 2-Propenoic acid, 3-[5-(4-nitrophenyl)-2-furanyl]-, (E)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of 2-Propenoic acid, 3-[5-(4-nitrophenyl)-2-furanyl]-, (E)-

Chemical Property:

PSA：96.26000
LogP:3.47580
XLogP3:2.5
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:3
Exact Mass:259.04807239
Heavy Atom Count:19
Complexity:368

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC(=CC=C1C2=CC=C(O2)C=CC(=O)O)[N+](=O)[O-]

Technology Process of 2-Propenoic acid, 3-[5-(4-nitrophenyl)-2-furanyl]-, (E)-

There total 7 articles about 2-Propenoic acid, 3-[5-(4-nitrophenyl)-2-furanyl]-, (E)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 938056-33-8
methyl (E)-3-[5-(4-nitrophenyl)-furan-2-yl]acrylate

: 62806-39-7,58110-34-2
3-<5-(4-Nitrophenyl)-2-furyl>propenoic acid

Guidance literature:: With sodium hydroxide; In methanol; at 0 - 80 ℃;
DOI:10.1021/jm061481l

Reference yield: 70.0%

: 141-82-2
malonic acid

: 7147-77-5
5-(4-nitrophenyl)-2-furaldehyde

: 62806-39-7,58110-34-2
3-<5-(4-Nitrophenyl)-2-furyl>propenoic acid

Guidance literature:: With piperidine; pyridine; for 4h; Heating;

Reference yield:

: 7147-77-5
5-(4-nitrophenyl)-2-furaldehyde

: 62806-39-7,58110-34-2
3-<5-(4-Nitrophenyl)-2-furyl>propenoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 89 percent / LiOH / tetrahydrofuran / 4 h / 20 °C

2: 91 percent / aq. NaOH / methanol / 0 - 80 °C

With lithium hydroxide; sodium hydroxide; In tetrahydrofuran; methanol; 1: Horner-Wadsworth-Emmons reaction;
DOI:10.1021/jm061481l