(3,4-Dichlorophenyl)(3-hydroxyphenyl)methanone

Base Information

Chemical Name:(3,4-Dichlorophenyl)(3-hydroxyphenyl)methanone
CAS No.:62810-54-2
Molecular Formula:C13H8Cl2O2
Molecular Weight:267.10700
Hs Code.:
DSSTox Substance ID:DTXSID60505304
Wikidata:Q82360311

Synonyms:62810-54-2;(3,4-Dichlorophenyl)(3-hydroxyphenyl)methanone;DTXSID60505304

Suppliers and Price of (3,4-Dichlorophenyl)(3-hydroxyphenyl)methanone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of (3,4-Dichlorophenyl)(3-hydroxyphenyl)methanone

Chemical Property:

Melting Point:140°C
PSA：37.30000
LogP:3.93000
XLogP3:4.7
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:265.9901349
Heavy Atom Count:17
Complexity:283

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC(=CC(=C1)O)C(=O)C2=CC(=C(C=C2)Cl)Cl

Technology Process of (3,4-Dichlorophenyl)(3-hydroxyphenyl)methanone

There total 1 articles about (3,4-Dichlorophenyl)(3-hydroxyphenyl)methanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2398-37-0
3-methoxyphenyl bromide

: 17274-10-1
sodium 3,4-dichlorobenzoate

: 62810-54-2
(3,4-Dichloro-phenyl)-(3-hydroxy-phenyl)-methanone

Guidance literature:: Multistep reaction; (i) nBuLi, (ii) /BRN= 4039878/, (iii) (demethylation);

Reference yield: 72.0%

: 62810-54-2
(3,4-Dichloro-phenyl)-(3-hydroxy-phenyl)-methanone

: 535-11-5,41978-69-2
Ethyl 2-bromopropionate

: 76981-51-6
2-[3-(3,4-Dichloro-benzoyl)-phenoxy]-propionic acid ethyl ester

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 80 ℃; for 4h;

Reference yield:

: 62810-54-2
(3,4-Dichloro-phenyl)-(3-hydroxy-phenyl)-methanone

: 76981-39-0
2-[3-(3,4-Dichloro-benzoyl)-phenoxy]-propionic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 72 percent / potassium carbonate / dimethylformamide / 4 h / 80 °C

2: 72 percent / 1.) H₂O, sodium carbonate, 2.) acid / ethanol / Ambient temperature

With water; sodium carbonate; potassium carbonate; In ethanol; N,N-dimethyl-formamide;