7,8,9,10-Tetrahydrophenanthridine

Base Information

Chemical Name:7,8,9,10-Tetrahydrophenanthridine
CAS No.:62833-92-5
Molecular Formula:C13H13N
Molecular Weight:183.253
Hs Code.:
DSSTox Substance ID:DTXSID50397174
Wikidata:Q82198285

Synonyms:7,8,9,10-tetrahydrophenanthridine;62833-92-5;Phenanthridine, 7,8,9,10-tetrahydro-;Oprea1_694807;SCHEMBL9155402;DTXSID50397174;OGJFULQWWMMHAA-UHFFFAOYSA-N;BBL003937;STK185991;AKOS005412247;CCG-314917;NCGC00341663-01;VS-01463;AB01333871-02

Suppliers and Price of 7,8,9,10-Tetrahydrophenanthridine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 7,8,9,10-Tetrahydrophenanthridine

Chemical Property:

XLogP3:3.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:0
Exact Mass:183.104799419
Heavy Atom Count:14
Complexity:201

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CCC2=C(C1)C=NC3=CC=CC=C23

Technology Process of 7,8,9,10-Tetrahydrophenanthridine

There total 1 articles about 7,8,9,10-Tetrahydrophenanthridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 19.0%

: 108-94-1,11119-77-0,9003-41-2,9075-99-4
cyclohexanone

: 5882-44-0
N,N-dimethylaniline hydrochloride

: 4-cyclohexyl-N-methylaniline

: 2-cyclohexyl-7,8,9,10-tetrahydro-phenanthridine

: 62833-92-5
7,8,9,10-tetrahydrophenanthridine

: N,N-dimethylamino-4-cyclohexylbenzene

Guidance literature:: In water; at 250 ℃; for 24h;
DOI:10.1016/j.tetlet.2005.07.165

Reference yield:

: 62833-92-5
7,8,9,10-tetrahydrophenanthridine

: 229-87-8
phenanthridine

Guidance literature:: With selenium; at 320 ℃;

Reference yield:

: 62833-92-5
7,8,9,10-tetrahydrophenanthridine

: 130012-93-0,130062-21-4
N-<(phenyloxy)carbonyl>-6a,10a-epoxy-6-ethynyl-10-hydroxy-5,6,6a,7,8,9,10,10a-octahydrophenanthridine

Guidance literature:: Multi-step reaction with 7 steps

1: 78 percent / mCPBA / CH₂Cl₂ / 1 h / 25 °C

2: 87 percent / 20 h / 100 °C

3: 100 percent / K₂CO₃ / methanol / 1 h / 25 °C

4: 92 percent / 2,6-lutidine / CH₂Cl₂ / 1 h / 0 °C

5: 1.) THF, -78 degC to 0 deg C, 2.) -78 deg C to 25 deg C, 1 h

6: 85 percent / mCPBA / CH₂Cl₂ / 2 h / 25 °C

7: 100 percent / Bu₄NF / tetrahydrofuran / 3 h / 42 °C

With 2,6-dimethylpyridine; tetrabutyl ammonium fluoride; potassium carbonate; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1021/ja00008a045