6-hydroxy-4-(4-hydroxy-3-methoxyphenyl)-3-(hydroxymethyl)-7-methoxy-1,2,3,4-tetrahydronaphthalene-2-carboxylic acid

Base Information

• Chemical Name: 6-hydroxy-4-(4-hydroxy-3-methoxyphenyl)-3-(hydroxymethyl)-7-methoxy-1,2,3,4-tetrahydronaphthalene-2-carboxylic acid
• CAS No.: 11041-15-9
• Molecular Formula: C₂₀H₂₂O₇
• Molecular Weight: 374.39
• Mol file: 11041-15-9.mol

Synonyms:2-Naphthalenecarboxylicacid, 1,2,3,4-tetrahydro-6-hydroxy-4-(4-hydroxy-3-methoxyphenyl)-3-(hydroxymethyl)-7-methoxy-,[2R-(2a,3b,4a)]-; a-Conidendric acid (8CI);Conidendric acid; NSC 32977

Chemical Property of 6-hydroxy-4-(4-hydroxy-3-methoxyphenyl)-3-(hydroxymethyl)-7-methoxy-1,2,3,4-tetrahydronaphthalene-2-carboxylic acid

Chemical Property:

• Vapor Pressure: 1.13E-16mmHg at 25°C
• Boiling Point: 628.7°Cat760mmHg
• Flash Point: 224.9°C
• Density: 1.355g/cm³

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 6-hydroxy-4-(4-hydroxy-3-methoxyphenyl)-3-(hydroxymethyl)-7-methoxy-1,2,3,4-tetrahydronaphthalene-2-carboxylic acid

There total 3 articles about 6-hydroxy-4-(4-hydroxy-3-methoxyphenyl)-3-(hydroxymethyl)-7-methoxy-1,2,3,4-tetrahydronaphthalene-2-carboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(7RS,8R,8'R)-4,4',7-trihydroxy-3,3'-dimethoxylignano-9,9'-lactone (347359-71-1) → C20H22O7 (11041-15-9)

Guidance literature:

With magnesium oxide; In water; isopropyl alcohol; at 69.84 ℃; for 4h;

DOI:10.1016/j.jcat.2011.05.025

Reference yield:

(7RS,8R,8'R)-4,4',7-trihydroxy-3,3'-dimethoxylignano-9,9'-lactone (347359-71-1) → α-conidendrin (518-55-8,5474-93-1,22614-13-7,26358-20-3,85699-62-3,89104-61-0,105817-20-7) + C20H22O7 (11041-15-9)

Guidance literature:

In water; isopropyl alcohol; at 69.84 ℃;

DOI:10.1016/j.jcat.2011.05.025

Reference yield:

conidendrin (518-55-8,5474-93-1,22614-13-7,26358-20-3,85699-62-3,89104-61-0,105817-20-7) → α-conidendric acid (11041-15-9)

Guidance literature:

Alkaline conditions;

DOI:10.1016/j.apcata.2014.12.051

upstream raw materials:

(7RS,8R,8'R)-4,4',7-trihydroxy-3,3'-dimethoxylignano-9,9'-lactone

conidendrin

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