Benzene, 1-decenyl-, (E)-

Base Information

Chemical Name:Benzene, 1-decenyl-, (E)-
CAS No.:62839-71-8
Molecular Formula:C16H24
Molecular Weight:216.367
Hs Code.:

Synonyms:

Suppliers and Price of Benzene, 1-decenyl-, (E)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Benzene, 1-decenyl-, (E)-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Benzene, 1-decenyl-, (E)-

There total 55 articles about Benzene, 1-decenyl-, (E)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 588-72-7,1340-14-3
[(E)-2-bromoethenyl]benzene

: 66217-56-9
4,4,5,5-tetramethyl-2-octyl-[1,3,2]dioxaborolane

: 62839-71-8
(E)-1-phenyl-1-decene

Guidance literature:: 4,4,5,5-tetramethyl-2-octyl-[1,3,2]dioxaborolane; With tetramethylenebis(magnesium chloride); In tetrahydrofuran; toluene; at 0 - 20 ℃; for 1h; Inert atmosphere;

[(E)-2-bromoethenyl]benzene; With tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; toluene; at 20 ℃; for 16h; Inert atmosphere;
DOI:10.1002/anie.201201704

Reference yield: 88.0%

: 2404-44-6
1,2-Epoxydecane

: 24388-23-6
2-phenyl-4,4,5,5-tetramethyl-1,3,2-dioxoborole

: 62839-71-8
(E)-1-phenyl-1-decene

Guidance literature:: With 2,2,6,6-tetramethyl-piperidine; n-butyllithium; In tetrahydrofuran; hexane; at -30 - 60 ℃; for 4.5h; Schlenk technique;
DOI:10.1021/acs.orglett.9b00517

Reference yield: 85.0%

: 30089-00-0
9-octyl-9-bora-bicyclo[3.3.1]nonane

: 588-72-7,1340-14-3
[(E)-2-bromoethenyl]benzene

: 62839-71-8
(E)-1-phenyl-1-decene

Guidance literature:: With sodium hydroxide; dihydrogen peroxide; cis-dichloro-1,1'-bis(diphenylphosphino)ferrocene palladium(II); In tetrahydrofuran; To a soln. of 9-octyl-9-BBN is added (C6H5)(CH)2Br, THF and aq. NaOH at room temp., mixt. refluxed overnight (14-16 h), react. mixt. diluted with hexane or benzene, residue oxidized by H2O2 at room temp.; Extracted, washed with brine, dried (MgSO4), final product (E/Z=99/1).;
DOI:10.1021/ja00183a048