3-(2-Nitrovinyl)-1-phenylindole

Base Information

Chemical Name:3-(2-Nitrovinyl)-1-phenylindole
CAS No.:63050-02-2
Molecular Formula:C16H12N2O2
Molecular Weight:264.27900
Hs Code.:2933990090
European Community (EC) Number:636-307-7
Nikkaji Number:J1.015.598C,J236.656H

Synonyms:3-(2-Nitrovinyl)-1-phenylindole;SCHEMBL9428072;JHTQRJSIADSEBT-ZHACJKMWSA-N;AKOS024319705;1H-Indole, 3-(2-nitroethenyl)-1-phenyl-;3-(2-NITROVINYL)-1-PHENYLINDOLE, 99%;3-[(E)-2-Nitroethenyl]-1-phenyl-1H-indole #

Suppliers and Price of 3-(2-Nitrovinyl)-1-phenylindole

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of 3-(2-Nitrovinyl)-1-phenylindole

Chemical Property:

PSA：50.75000
LogP:4.40110
XLogP3:3.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:264.089877630
Heavy Atom Count:20
Complexity:371

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:Xn
Statements: 22-37/38-41
Safety Statements: 26-36/37/39

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)N2C=C(C3=CC=CC=C32)C=C[N+](=O)[O-]
Isomeric SMILES:C1=CC=C(C=C1)N2C=C(C3=CC=CC=C32)/C=C/[N+](=O)[O-]

Technology Process of 3-(2-Nitrovinyl)-1-phenylindole

There total 5 articles about 3-(2-Nitrovinyl)-1-phenylindole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 83-72-7
2-hydroxynaphtho-1,4-quinone

: 102-96-5
(2-nitroethenyl)benzene

: 63050-02-2
3-(2-nitrovinyl)-1-phenyl-1H-indole

Guidance literature:: In water; at 80 ℃; for 12h;
DOI:10.1016/j.tetlet.2009.06.107

Reference yield:

: 591-50-4
iodobenzene

: 63050-02-2
3-(2-nitrovinyl)-1-phenyl-1H-indole

Guidance literature:: Multi-step reaction with 2 steps

1: copper(I) oxide; potassium carbonate / N,N-dimethyl-formamide / 72 h / 130 °C

2: ammonium acetate / 100 °C

With copper(I) oxide; ammonium acetate; potassium carbonate; In N,N-dimethyl-formamide;
DOI:10.1021/acs.orglett.8b03019