2-(Sodiooxy)-1-cyclopentene-1-carboxylic acid methyl ester

Base Information

• Chemical Name: 2-(Sodiooxy)-1-cyclopentene-1-carboxylic acid methyl ester
• CAS No.: 63178-03-0
• Molecular Formula: C7H10O3.Na
• Molecular Weight: 164.136

Synonyms:2-methoxycarbonyl-cyclopent-1-enolate;sodium salt of 2-carbomethoxycyclopentanone;2-carbomethoxycyclopentanone;Sodium;2-sodio-2-carbomethoxycyclopentanone;

Chemical Property of 2-(Sodiooxy)-1-cyclopentene-1-carboxylic acid methyl ester

Chemical Property:

• PSA: 49.36000
• LogP: 1.02790

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-(Sodiooxy)-1-cyclopentene-1-carboxylic acid methyl ester

There total 1 articles about 2-(Sodiooxy)-1-cyclopentene-1-carboxylic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methyl 2-oxocyclopentane-1-carboxylate (10472-24-9,265317-94-0) → methyl 2-hydroxycyclopentene-1-carboxylate sodium salt (63178-03-0)

Guidance literature:

With sodium hydride; In diethyl ether; mineral oil; at 0 - 20 ℃; Inert atmosphere;

DOI:10.1021/ol201661s

Reference yield: 82.0%

2-methylenecyclohexyl acetate (53723-50-5) + methyl 2-hydroxycyclopentene-1-carboxylate sodium salt (63178-03-0) → methyl 1-(1-cyclohexenylmethyl)-2-oxocyclopentanecarboxylate (82352-45-2)

Guidance literature:

hexacarbonyl molybdenum; In toluene; for 6h; Heating;

DOI:10.1021/ja00384a071

Reference yield: 60.0%

methyl 2-hydroxycyclopentene-1-carboxylate sodium salt (63178-03-0) + Carbonic acid (E)-4-methoxycarbonyloxy-4-phenyl-but-2-enyl ester methyl ester (107174-76-5) → 2-((E)-4-Methoxycarbonyloxy-1-phenyl-but-2-enyloxy)-cyclopent-1-enecarboxylic acid methyl ester (107174-79-8)

Guidance literature:

W(O);

DOI:10.1021/ja00241a043

upstream raw materials:

methyl 2-oxocyclopentane-1-carboxylate

Downstream raw materials:

methyl 1-(3-phenyl-2-propenyl)-2-oxocyclopentanecarboxylate

methyl 1-(1-phenyl-2-propenyl)-2-oxocyclopentanecarboxylate

methyl 1-(1-cyclohexenylmethyl)-2-oxocyclopentanecarboxylate

(1S,5S)-5-(1-Methoxycarbonyl-2-oxo-cyclopentyl)-cyclohex-3-enecarboxylic acid methyl ester

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