Cyclohexanol, 3-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-5-[[(1,1-dimethylethyl)diphenylsil yl]oxy]-2-[(2-methoxyethoxy)methoxy]-2-(2-propenyl)-, (1S,2R,3S,5S)-

Base Information

Chemical Name:Cyclohexanol, 3-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-5-[[(1,1-dimethylethyl)diphenylsil yl]oxy]-2-[(2-methoxyethoxy)methoxy]-2-(2-propenyl)-, (1S,2R,3S,5S)-
CAS No.:631900-24-8
Molecular Formula:C35H56O6Si2
Molecular Weight:628.997
Hs Code.:

Cyclohexanol,
3-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-5-[[(1,1-dimethylethyl)diphenylsil
yl]oxy]-2-[(2-methoxyethoxy)methoxy]-2-(2-propenyl)-, (1S,2R,3S,5S)-

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Cyclohexanol, 3-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-5-[[(1,1-dimethylethyl)diphenylsil yl]oxy]-2-[(2-methoxyethoxy)methoxy]-2-(2-propenyl)-, (1S,2R,3S,5S)-

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Technology Process of Cyclohexanol, 3-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-5-[[(1,1-dimethylethyl)diphenylsil yl]oxy]-2-[(2-methoxyethoxy)methoxy]-2-(2-propenyl)-, (1S,2R,3S,5S)-

There total 5 articles about Cyclohexanol, 3-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-5-[[(1,1-dimethylethyl)diphenylsil yl]oxy]-2-[(2-methoxyethoxy)methoxy]-2-(2-propenyl)-, (1S,2R,3S,5S)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: C₃₈H₆₄O₆Si₃

: 631900-24-8
(1S,2R,3S,5S)-2-allyl-3-(tert-butyldimethylsilanyloxy)-5-(tert-butyldiphenylsilyloxy)-2-(2-methoxyethoxymethoxy)cyclohexanol

Guidance literature:: With potassium carbonate; In methanol; at 20 ℃; for 12h;
DOI:10.1002/anie.200351455

Reference yield: 95.0%

: 631900-13-5
(1R,2S,4S,6S)-1-allyl-1-(2-methoxyethoxymethoxy)-2-(tert-butyldimethylsilyloxy)-4-(tert-butyldiphenylsilyloxy)-6-trimethylsilyloxycyclohexane

: 631900-24-8
(1S,2R,3S,5S)-2-allyl-3-(tert-butyldimethylsilanyloxy)-5-(tert-butyldiphenylsilyloxy)-2-(2-methoxyethoxymethoxy)cyclohexanol

Guidance literature:: With potassium carbonate; In methanol; at 20 ℃; for 12h;
DOI:10.1002/chem.200500640

Reference yield:

: (2S,4S,6S)-1-allyl-2-(tert-butyldimethylsilyloxy)-4-(tert-butyldiphenylsilyloxy)-6-trimethylsilyloxycyclohexanol

: 631900-24-8
(1S,2R,3S,5S)-2-allyl-3-(tert-butyldimethylsilanyloxy)-5-(tert-butyldiphenylsilyloxy)-2-(2-methoxyethoxymethoxy)cyclohexanol

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / (i-Pr)2NEt / 1,2-dichloro-ethane / 8 h / 70 °C

2: 95 percent / K₂CO₃ / methanol / 12 h / 20 °C

With potassium carbonate; N-ethyl-N,N-diisopropylamine; In methanol; 1,2-dichloro-ethane;
DOI:10.1002/chem.200500640