2,4-Dinitrophenylhydrazone mesityl oxide

Base Information

Chemical Name:2,4-Dinitrophenylhydrazone mesityl oxide
CAS No.:964-83-0
Molecular Formula:C12H14N4O4
Molecular Weight:278.268
Hs Code.:
NSC Number:404137
DSSTox Substance ID:DTXSID20429835

Synonyms:2,4-dinitrophenylhydrazone mesityl oxide;964-83-0;NSC404137;DTXSID20429835;STK524799;AKOS001011421;NSC-404137;SR-01000033371;SR-01000033371-1;Z56834202;(2E)-1-(2,4-dinitrophenyl)-2-(4-methylpent-3-en-2-ylidene)hydrazine

Suppliers and Price of 2,4-Dinitrophenylhydrazone mesityl oxide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 7 raw suppliers

Chemical Property of 2,4-Dinitrophenylhydrazone mesityl oxide

Chemical Property:

Vapor Pressure:7.86E-07mmHg at 25°C
Boiling Point:406.9°C at 760 mmHg
Flash Point:199.9°C
Density:1.29g/cm³
XLogP3:4.5
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:3
Exact Mass:278.10150494
Heavy Atom Count:20
Complexity:432

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC(=CC(=NNC1=C(C=C(C=C1)[N+](=O)[O-])[N+](=O)[O-])C)C
Isomeric SMILES:CC(=C/C(=N/NC1=C(C=C(C=C1)[N+](=O)[O-])[N+](=O)[O-])/C)C

Technology Process of 2,4-Dinitrophenylhydrazone mesityl oxide

There total 11 articles about 2,4-Dinitrophenylhydrazone mesityl oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 563-80-4
3-methyl-butan-2-one

: 964-83-0
4-methyl-3-penten-2-one (2,4-dinitrophenyl)hydrazone

Guidance literature:: Multi-step reaction with 5 steps

1: 87 percent / p-toluenosulfonic acid / 1.) o deg C, 30 min., 2.) room temp., overnight

2: 4.5 g / p-toluenesulfonic acid / Heating

3: 76 percent / potassium t-butoxide / pentane / 1.) 0 deg C, 30 min., 2.) 2 h, room temp.

4: MeLi / diethyl ether / 1.) 0 deg C, 0.5 h, 2.) 2 h, room temp.

5: methanol; CCl₄

With potassium tert-butylate; methyllithium; toluene-4-sulfonic acid; toluene-4-sulfonic acid; In methanol; tetrachloromethane; diethyl ether; pentane;

Reference yield:

: 97-00-7
1-chloro-2,4-dinitro-benzene

: 964-83-0
4-methyl-3-penten-2-one (2,4-dinitrophenyl)hydrazone

Guidance literature:: Multi-step reaction with 2 steps

1: diluted alcohol

With ethanol;

Reference yield:

: 51334-68-0
1,1-dichloro-2-methoxy-3,3-dimethylcyclopropane

: 964-83-0
4-methyl-3-penten-2-one (2,4-dinitrophenyl)hydrazone

Guidance literature:: Multi-step reaction with 2 steps

1: hexamethylphosphoramide / diethyl ether; tetrahydrofuran / 1.) -65 deg C, 1.5 h, 2.) RT, overnight

2: methanol; CCl₄

With N,N,N,N,N,N-hexamethylphosphoric triamide; In tetrahydrofuran; methanol; tetrachloromethane; diethyl ether;