9-[2,3-o-(1-Methylethylidene)-5-o-tritylpentofuranosyl]-9h-purin-6-amine

Base Information

• Chemical Name: 9-[2,3-o-(1-Methylethylidene)-5-o-tritylpentofuranosyl]-9h-purin-6-amine
• CAS No.: 10299-43-1
• Molecular Formula: C32H31N5O4
• Molecular Weight: 549.6196
• NSC Number: 90386
• DSSTox Substance ID: DTXSID30293524
• Mol file: 10299-43-1.mol

Synonyms:NSC90386;9-[2,3-o-(1-methylethylidene)-5-o-tritylpentofuranosyl]-9h-purin-6-amine;DTXSID30293524;NSC-90386

Chemical Property of 9-[2,3-o-(1-Methylethylidene)-5-o-tritylpentofuranosyl]-9h-purin-6-amine

Chemical Property:

• Vapor Pressure: 7.13E-21mmHg at 25°C
• Boiling Point: 725°Cat760mmHg
• Flash Point: 392.3°C
• Density: 1.36g/cm³
• XLogP3: 4.3
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 8
• Rotatable Bond Count: 7
• Exact Mass: 549.23760449
• Heavy Atom Count: 41
• Complexity: 829

Purity/Quality:

85.0-99.8% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1(OC2C(OC(C2O1)N3C=NC4=C(N=CN=C43)N)COC(C5=CC=CC=C5)(C6=CC=CC=C6)C7=CC=CC=C7)C

Technology Process of 9-[2,3-o-(1-Methylethylidene)-5-o-tritylpentofuranosyl]-9h-purin-6-amine

There total 2 articles about 9-[2,3-o-(1-Methylethylidene)-5-o-tritylpentofuranosyl]-9h-purin-6-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

trityl chloride (76-83-5) + 2',3'-isopropylidene adenosine (362-75-4) → O2',O3'-isopropylidene-O5'-trityl-adenosine (10299-43-1)

Guidance literature:

With pyridine; at 60 ℃; for 12h;

DOI:10.1016/j.tetlet.2010.03.103

Reference yield:

→ O2',O3'-isopropylidene-O5'-trityl-adenosine (10299-43-1)

Guidance literature:

2',3'-Isopropyliden-adenosin, Tritylchlorid, Pyridin;

Reference yield:

di-tert-butyl dicarbonate (24424-99-5) + O2',O3'-isopropylidene-O5'-trityl-adenosine (10299-43-1) → C42H47N5O8

Guidance literature:

With dmap; In tetrahydrofuran; at 20 ℃; for 16h;

DOI:10.1016/j.tetlet.2010.03.103

upstream raw materials:

trityl chloride

2',3'-isopropylidene adenosine

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