1,2,3,4-Tetrahydro-2-methyl-1,4-ethanoisoquinoline

Base Information

Chemical Name:1,2,3,4-Tetrahydro-2-methyl-1,4-ethanoisoquinoline
CAS No.:63385-90-0
Molecular Formula:C12H15N
Molecular Weight:173.25400
Hs Code.:

Synonyms:2-methyl-5,6-benzo-2-azabicyclo<2.2.2>octane;2-methyl-1,2,3,4-tetrahydro-1,4-ethano-isoquinoline;

Suppliers and Price of 1,2,3,4-Tetrahydro-2-methyl-1,4-ethanoisoquinoline

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 1,2,3,4-Tetrahydro-2-methyl-1,4-ethanoisoquinoline

Chemical Property:

PSA：3.24000
LogP:2.48840

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1,2,3,4-Tetrahydro-2-methyl-1,4-ethanoisoquinoline

There total 6 articles about 1,2,3,4-Tetrahydro-2-methyl-1,4-ethanoisoquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 3118-05-6
2-methyl-5,6-benzo-2-azabicyclo<2.2.2>octan-3-one

: 63385-90-0
2-methyl-5,6-benzo-2-azabicyclo<2.2.2>octane

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether; Heating;
DOI:10.1016/S0040-4020(01)91227-X

Reference yield:

: 694-85-9,859803-97-7
1-methyl-2-pyridone

: 63385-90-0
2-methyl-5,6-benzo-2-azabicyclo<2.2.2>octane

Guidance literature:: Multi-step reaction with 3 steps

1: 10 percent / CH₂Cl₂; toluene

2: 91 percent / H₂ / Pd/C / diethyl ether / 6 h

3: 91 percent / LiAlH₄ / diethyl ether / Heating

With lithium aluminium tetrahydride; hydrogen; palladium on activated charcoal; In diethyl ether; dichloromethane; toluene;
DOI:10.1016/S0040-4020(01)91227-X

Reference yield:

: 1608-42-0
benzenedizolium-2-carboxylate

: 63385-90-0
2-methyl-5,6-benzo-2-azabicyclo<2.2.2>octane

Guidance literature:: Multi-step reaction with 3 steps

1: 10 percent / CH₂Cl₂; toluene

2: 91 percent / H₂ / Pd/C / diethyl ether / 6 h

3: 91 percent / LiAlH₄ / diethyl ether / Heating

With lithium aluminium tetrahydride; hydrogen; palladium on activated charcoal; In diethyl ether; dichloromethane; toluene;
DOI:10.1016/S0040-4020(01)91227-X