Technology Process of 1-Benzyl-2-(4-bromobutoxy)benzene
There total 5 articles about 1-Benzyl-2-(4-bromobutoxy)benzene which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium carbonate;
In
N,N-dimethyl-formamide;
at 60 ℃;
for 2h;
DOI:10.1002/anie.202014244
- Guidance literature:
-
Multi-step reaction with 3 steps
1: (1,2-dimethoxyethane)dichloronickel(II); 4,4'-di-tert-butyl-2,2'-bipyridine; potassium carbonate; lithium perchlorate / N,N-dimethyl-formamide / 20 °C / Electrochemical reaction; Inert atmosphere; Glovebox
2: trifluoroacetic acid / dichloromethane / 0.5 h / 20 °C
3: potassium carbonate / N,N-dimethyl-formamide / 2 h / 60 °C
With
(1,2-dimethoxyethane)dichloronickel(II); lithium perchlorate; potassium carbonate; trifluoroacetic acid; 4,4'-di-tert-butyl-2,2'-bipyridine;
In
dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/anie.202014244
- Guidance literature:
-
Multi-step reaction with 2 steps
1: trifluoroacetic acid / dichloromethane / 0.5 h / 20 °C
2: potassium carbonate / N,N-dimethyl-formamide / 2 h / 60 °C
With
potassium carbonate; trifluoroacetic acid;
In
dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/anie.202014244
