9H-Fluorene, 2,7-dibromo-9,9-bis[4-(octyloxy)phenyl]-

Base Information

Chemical Name:9H-Fluorene, 2,7-dibromo-9,9-bis[4-(octyloxy)phenyl]-
CAS No.:634558-40-0
Molecular Formula:C41H48Br2O2
Molecular Weight:732.639
Hs Code.:

Synonyms:9,9-bis(4-octyloxyphenyl)-2,7-dibromofluorene;2,7-dibromo-9,9-bis(4-(octyloxy)phenyl)-9H-fluorene;2,7-dibromo-9,9-bis(4-octyloxyphenyl)fluorene;9H-Fluorene,2,7-dibromo-9,9-bis[4-(octyloxy)phenyl];

Suppliers and Price of 9H-Fluorene, 2,7-dibromo-9,9-bis[4-(octyloxy)phenyl]-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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Total 1 raw suppliers

Chemical Property of 9H-Fluorene, 2,7-dibromo-9,9-bis[4-(octyloxy)phenyl]-

Chemical Property:

PSA：18.46000
LogP:13.05330

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 9H-Fluorene, 2,7-dibromo-9,9-bis[4-(octyloxy)phenyl]-

There total 4 articles about 9H-Fluorene, 2,7-dibromo-9,9-bis[4-(octyloxy)phenyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 111-83-1
1-bromo-octane

: 169169-89-5
4,4'-(2,7-dibromo-9H-fluorene-9,9-diyl)diphenol

: 634558-40-0
2,7-dibromo-9,9-bis(4-(octyloxy)phenyl)-9H-fluorene

Guidance literature:: With potassium hydroxide; In ethanol; at 80 ℃; for 20h;
DOI:10.1016/j.reactfunctpolym.2012.01.002

Reference yield: 64.0%

: 629-27-6
1-Iodooctane

: 169169-89-5
4,4'-(2,7-dibromo-9H-fluorene-9,9-diyl)diphenol

: 634558-40-0
2,7-dibromo-9,9-bis(4-(octyloxy)phenyl)-9H-fluorene

Guidance literature:: With potassium hydroxide; In cyclohexanol; at 120 - 130 ℃; for 14h;
DOI:10.1039/b700047b

Reference yield:

: 14348-75-5
2,7-dibromofluorene-9-one

: 634558-40-0
2,7-dibromo-9,9-bis(4-(octyloxy)phenyl)-9H-fluorene

Guidance literature:: Multi-step reaction with 2 steps

1: HCl; ZnCl₂

2: KI; K₂CO₃ / acetone

With hydrogenchloride; potassium carbonate; potassium iodide; zinc(II) chloride; In acetone;
DOI:10.1039/b309006j