1-Piperazinecarboxylic acid, 4-[7-(2-butynyl)-2-chloro-1-[(2-cyanophenyl)methyl]-6,7-dihydro-6-oxo-1 H-purin-8-yl]-, 1,1-dimethylethyl ester

Base Information

Chemical Name:1-Piperazinecarboxylic acid, 4-[7-(2-butynyl)-2-chloro-1-[(2-cyanophenyl)methyl]-6,7-dihydro-6-oxo-1 H-purin-8-yl]-, 1,1-dimethylethyl ester
CAS No.:635722-61-1
Molecular Formula:C26H28ClN7O3
Molecular Weight:522.006
Hs Code.:

1-Piperazinecarboxylic acid,
4-[7-(2-butynyl)-2-chloro-1-[(2-cyanophenyl)methyl]-6,7-dihydro-6-oxo-1
H-purin-8-yl]-, 1,1-dimethylethyl ester

Synonyms:

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Chemical Property of 1-Piperazinecarboxylic acid, 4-[7-(2-butynyl)-2-chloro-1-[(2-cyanophenyl)methyl]-6,7-dihydro-6-oxo-1 H-purin-8-yl]-, 1,1-dimethylethyl ester

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Technology Process of 1-Piperazinecarboxylic acid, 4-[7-(2-butynyl)-2-chloro-1-[(2-cyanophenyl)methyl]-6,7-dihydro-6-oxo-1 H-purin-8-yl]-, 1,1-dimethylethyl ester

There total 1 articles about 1-Piperazinecarboxylic acid, 4-[7-(2-butynyl)-2-chloro-1-[(2-cyanophenyl)methyl]-6,7-dihydro-6-oxo-1 H-purin-8-yl]-, 1,1-dimethylethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 635722-60-0
t-Butyl 4-[7-(2-butynyl)-2-chloro-6-oxo-6,7-dihydro-1H-purin-8-yl]piperazine-1-carboxylate

: 22115-41-9
2-(bromomethyl)benzonitrile

: 635722-61-1
t-Butyl 4-[7-(2-butynyl)-2-chloro-1-(2-cyanobenzyl)-6-oxo-6,7-dihydro-1H-purin-8-yl]piperazine-1-carboxylate

Guidance literature:: With potassium carbonate; In hexane; water; ethyl acetate; N,N-dimethyl-formamide;

Reference yield:

: 635722-61-1
t-Butyl 4-[7-(2-butynyl)-2-chloro-1-(2-cyanobenzyl)-6-oxo-6,7-dihydro-1H-purin-8-yl]piperazine-1-carboxylate

: 933-90-4
3-hydroxypyridine-2-carboxamide

: C₃₂H₃₃N₉O₅

Guidance literature:: With potassium carbonate; In 1-methyl-pyrrolidin-2-one; at 100 ℃; for 2h;

Reference yield:

: 635722-61-1
t-Butyl 4-[7-(2-butynyl)-2-chloro-1-(2-cyanobenzyl)-6-oxo-6,7-dihydro-1H-purin-8-yl]piperazine-1-carboxylate

: 933-90-4
3-hydroxypyridine-2-carboxamide

: 76-05-1
trifluoroacetic acid

: 3-[7-(2-butynyl)-1-(2-cyanobenzyl)-6-oxo-8-(piperazin-1-yl)-6,7-dihydro-1H-purin-2-yloxy]pyridine-2-carboxylic amide trifluoroacetate

Guidance literature:: t-Butyl 4-[7-(2-butynyl)-2-chloro-1-(2-cyanobenzyl)-6-oxo-6,7-dihydro-1H-purin-8-yl]piperazine-1-carboxylate; 3-hydroxypyridine-2-carboxamide; With potassium carbonate; In 1-methyl-pyrrolidin-2-one; at 100 ℃; for 2h;

trifluoroacetic acid;