Benzenesulfonyl chloride, 4-[(trifluoromethyl)sulfonyl]-

Base Information

• Chemical Name: Benzenesulfonyl chloride, 4-[(trifluoromethyl)sulfonyl]-
• CAS No.: 63647-64-3
• Molecular Formula: C7H4ClF3O4S2
• Molecular Weight: 308.687

Synonyms:p-Trifluormethylsulfonylphenylsulfonylchlorid;p-Chlorsulfonylphenyltrifluormethylensulfon;

Chemical Property of Benzenesulfonyl chloride, 4-[(trifluoromethyl)sulfonyl]-

Chemical Property:

• PSA: 85.04000
• LogP: 4.06920

Purity/Quality:

99% ^*data from raw suppliers

4-((Trifluoromethyl)sulfonyl)benzenesulfonylchloride ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Benzenesulfonyl chloride, 4-[(trifluoromethyl)sulfonyl]-

There total 1 articles about Benzenesulfonyl chloride, 4-[(trifluoromethyl)sulfonyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

4-(trifluoromethanesulfonyl)aniline (473-27-8) → 4-((trifluoromethyl)sulfonyl)benzene-1-sulfonyl chloride (63647-64-3)

Guidance literature:

4-(trifluoromethanesulfonyl)aniline; With hydrogenchloride; In water;

With sodium nitrite; In water; for 0.25h;

With sulfur dioxide; copper(l) chloride; In water; at 0 ℃; for 0.5h;

Reference yield: 57.0%

2-piperidin-1-yl-phenylamine (39643-31-7) + 4-((trifluoromethyl)sulfonyl)benzene-1-sulfonyl chloride (63647-64-3) → N-(2-(piperidin-1-yl)phenyl)-4-((trifluoromethyl)sulfonyl)benzenesulfonamide

Guidance literature:

With pyridine; at 115 ℃; for 1h; Microwave irradiation;

Reference yield: 21.0%

2-morpholinoaniline (5585-33-1) + 4-((trifluoromethyl)sulfonyl)benzene-1-sulfonyl chloride (63647-64-3) → N-(2-morpholinophenyl)-4-((trifluoromethyl)sulfonyl)benzenesulfonamide

Guidance literature:

With pyridine; at 115 ℃; for 1h; Microwave irradiation;

upstream raw materials:

4-(trifluoromethanesulfonyl)aniline

Downstream raw materials:

5-phenyl-1-({4-[(trifluoromethyl)sulfonyl]phenyl}sulfonyl)-1H-pyrrole-3-carbaldehyde

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