Technology Process of 2-Naphthalenamine,
N,N-dibutyl-5-[2-[2-(methoxymethyl)phenyl]ethenyl]-
There total 6 articles about 2-Naphthalenamine,
N,N-dibutyl-5-[2-[2-(methoxymethyl)phenyl]ethenyl]- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
6-N,N-dibutylaminonaphthyl-(1)-methyltriphenylphosphonium bromide;
With
sodium methylate;
In
methanol;
at 60 ℃;
for 3h;
2-[(methoxymethyl)methyl]benzaldehyde;
In
methanol;
Heating;
DOI:10.1021/jp0345809
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: 77 percent / K2CO3 / dimethylformamide / 48 h / 130 °C
2.1: 78 percent / pyridine / 72 h / 220 °C
3.1: 100 percent / NaOH / pentan-1-ol / 72 h / 170 °C
4.1: LiAlH4 / diethyl ether
5.1: 13.2 g / PBr3
6.1: 99 percent / 7 h / Heating
7.1: NaOMe / methanol / 3 h / 60 °C
7.2: 61 percent / methanol / Heating
With
pyridine; sodium hydroxide; lithium aluminium tetrahydride; sodium methylate; phosphorus tribromide; potassium carbonate;
In
methanol; diethyl ether; pentan-1-ol; N,N-dimethyl-formamide;
DOI:10.1021/jp0345809
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: 100 percent / NaOH / pentan-1-ol / 72 h / 170 °C
2.1: LiAlH4 / diethyl ether
3.1: 13.2 g / PBr3
4.1: 99 percent / 7 h / Heating
5.1: NaOMe / methanol / 3 h / 60 °C
5.2: 61 percent / methanol / Heating
With
sodium hydroxide; lithium aluminium tetrahydride; sodium methylate; phosphorus tribromide;
In
methanol; diethyl ether; pentan-1-ol;
DOI:10.1021/jp0345809