Benzaldehyde, 2-[[2-(hydroxymethyl)phenyl]thio]-

Base Information

Chemical Name:Benzaldehyde, 2-[[2-(hydroxymethyl)phenyl]thio]-
CAS No.:63744-05-8
Molecular Formula:C₁₄H₁₂O₂S
Molecular Weight:244.314
Hs Code.:
DSSTox Substance ID:DTXSID80465138
Nikkaji Number:J1.953.949K
Wikidata:Q82290865

Synonyms:63744-05-8;Benzaldehyde, 2-[[2-(hydroxymethyl)phenyl]thio]-;DTXSID80465138;AKOS005064328

Suppliers and Price of Benzaldehyde, 2-[[2-(hydroxymethyl)phenyl]thio]-

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Chemical Property of Benzaldehyde, 2-[[2-(hydroxymethyl)phenyl]thio]-

Chemical Property:

XLogP3:2.6
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:4
Exact Mass:244.05580079
Heavy Atom Count:17
Complexity:244

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC=C(C(=C1)CO)SC2=CC=CC=C2C=O

Technology Process of Benzaldehyde, 2-[[2-(hydroxymethyl)phenyl]thio]-

There total 3 articles about Benzaldehyde, 2-[[2-(hydroxymethyl)phenyl]thio]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4521-31-7
o-hydroxymethyl thiophenol

: 89-98-5
2-chloro-benzaldehyde

: 63744-05-8
2-(2-hydroxymethylphenylthio)benzaldehyde

Guidance literature:: With sodium hydroxide; In N,N,N,N,N,N-hexamethylphosphoric triamide; water; at 100 ℃; for 7h;
DOI:10.1135/cccc19831187

Reference yield:

: 147-93-3
Thiosalicylic acid

: 63744-05-8
2-(2-hydroxymethylphenylthio)benzaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: LiAlH₄ / tetrahydrofuran / 24 h / 20 °C

2: aq. NaOH / hexamethylphosphoric acid triamide / 5 h / 100 °C

With sodium hydroxide; lithium aluminium tetrahydride; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide;
DOI:10.1248/cpb.51.1307