(4-Nitrophenyl)methyl (triphenyl-lambda~5~-phosphanylidene)acetate

Base Information

Chemical Name:(4-Nitrophenyl)methyl (triphenyl-lambda~5~-phosphanylidene)acetate
CAS No.:63760-39-4
Molecular Formula:C27H22NO4P
Molecular Weight:455.45
Hs Code.:
DSSTox Substance ID:DTXSID30602910
Wikidata:Q82500117

Synonyms:SCHEMBL10636434;DTXSID30602910;(4-Nitrophenyl)methyl (triphenyl-lambda~5~-phosphanylidene)acetate

Suppliers and Price of (4-Nitrophenyl)methyl (triphenyl-lambda~5~-phosphanylidene)acetate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 0 raw suppliers

Chemical Property of (4-Nitrophenyl)methyl (triphenyl-lambda~5~-phosphanylidene)acetate

Chemical Property:

XLogP3:5.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:7
Exact Mass:455.12864518
Heavy Atom Count:33
Complexity:639

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)P(=CC(=O)OCC2=CC=C(C=C2)[N+](=O)[O-])(C3=CC=CC=C3)C4=CC=CC=C4

Technology Process of (4-Nitrophenyl)methyl (triphenyl-lambda~5~-phosphanylidene)acetate

There total 3 articles about (4-Nitrophenyl)methyl (triphenyl-lambda~5~-phosphanylidene)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 16869-24-2
4-nitrobenzyl bromoacetate

: 603-35-0
triphenylphosphine

: 63760-39-4
(p-Nitrobenzyloxycarbonylmethylene)triphenylphosphorane

Guidance literature:: 4-nitrobenzyl bromoacetate; triphenylphosphine; In toluene; at 20 ℃;

With sodium hydroxide; In dichloromethane; water;
DOI:10.1002/anie.201916471

Reference yield:

: 619-73-8
4-nitrobenzyl chloride

: 63760-39-4
(p-Nitrobenzyloxycarbonylmethylene)triphenylphosphorane

Guidance literature:: Multi-step reaction with 2 steps

1: dicyclohexyl-carbodiimide; dmap / dichloromethane / 20 °C

2: toluene / 20 °C

With dmap; dicyclohexyl-carbodiimide; In dichloromethane; toluene;
DOI:10.1002/anie.201916471