Phenol, 4-methoxy-, thallium(1+) salt

Base Information

Chemical Name:Phenol, 4-methoxy-, thallium(1+) salt
CAS No.:63766-85-8
Molecular Formula:C₇H₇O₂*Tl
Molecular Weight:327.514
Hs Code.:

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Chemical Property of Phenol, 4-methoxy-, thallium(1+) salt

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Technology Process of Phenol, 4-methoxy-, thallium(1+) salt

There total 2 articles about Phenol, 4-methoxy-, thallium(1+) salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 20398-06-5
thallium (I) ethoxide

: 150-76-5
4-methoxy-phenol

: 63766-85-8
thallium 4-methoxyphenoxide

Guidance literature:: In tetrahydrofuran; pentane; phenol was dissolved in pentane and minimumamt. THF and treated with soln. thallium ethoxide in pentane, mixt. was stirred for 2 h; solid was filtered off, washed with pentane and dried in vacuo; elem. anal.;
DOI:10.1021/ic010615c

Reference yield:

: 63766-85-8
thallium 4-methoxyphenoxide

Guidance literature:: p-Methoxy-phenol und Tl-aethylat;
DOI:10.1021/ja01011a040

Reference yield: 83.0%

: W(=C₈H₁₂=C₈H₁₂=N-2,6-diisopropylphenyl)(N-2,6-diisopropylphenyl)Cl₂

: 63766-85-8
thallium 4-methoxyphenoxide

: W(OC₆H₄OCH₃)2((C₈H₁₂)2NC₆H₃(CH(CH₃)2)2)(NC₆H₃(CH(CH₃)2)2)

Guidance literature:: In tetrahydrofuran; diethyl ether; byproducts: TlCl; under N2; TlOC6H4OMe added to frozen soln. of W complex in Et2O-THF; warmed to room temp.; stirred for 2 h; volatiles removed in vac.; dissolved in small amt. of pentane; soln. filtered through Celite; crystd. from min. amt. of pentane at -35°C;recrystd. from pentane; elem. anal.;
DOI:10.1021/ic8014964