1,1-Diethoxytridec-2-yne

Base Information

Chemical Name:1,1-Diethoxytridec-2-yne
CAS No.:94088-24-1
Molecular Formula:C17H32 O2
Molecular Weight:268.44
Hs Code.:2911000000
European Community (EC) Number:302-022-9
DSSTox Substance ID:DTXSID20240466
Nikkaji Number:J288.530A
Wikidata:Q83123342
Mol file:94088-24-1.mol

Synonyms:1,1-Diethoxytridec-2-yne;94088-24-1;EINECS 302-022-9;1,1-Diethoxy-2-tridecyne;DTXSID20240466

Suppliers and Price of 1,1-Diethoxytridec-2-yne

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 1,1-Diethoxytridec-2-yne

Chemical Property:

Vapor Pressure:9.26E-05mmHg at 25°C
Boiling Point:349.8°Cat760mmHg
Flash Point:111.7°C
PSA：18.46000
Density:0.878g/cm³
LogP:4.91970
XLogP3:6.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:12
Exact Mass:268.240230259
Heavy Atom Count:19
Complexity:230

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCCCCCCCCCC#CC(OCC)OCC

Technology Process of 1,1-Diethoxytridec-2-yne

There total 4 articles about 1,1-Diethoxytridec-2-yne which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 10160-87-9
Propiolaldehyde diethyl acetal

: 112-29-8
1-bromo dodecane

: 94088-24-1
1,1-diethoxy-tridec-2-yne

Guidance literature:: With methyllithium lithium bromide; dimethyl sulfoxide; Yield given. Multistep reaction; 1.) 0 deg C, THF, ether, 15 min 2.) from 0 deg C to room temperature, stiring at room temperature 3h;
DOI:10.1016/S0040-4039(00)85233-8

Reference yield:

: 112-29-8
1-bromo dodecane

: 94088-24-1
1,1-diethoxy-tridec-2-yne

Guidance literature:: Multi-step reaction with 2 steps

1: liquid ammonia; dimethylformamide / nach Entfernung des Ammoniaks bei 65-70grad

2: diethyl ether / und anschliessend mit Orthoameisensaeure-triaethylester

With diethyl ether; ammonia; N,N-dimethyl-formamide;
DOI:10.1002/hlca.19590420202