N-P-(Chlorophenyl)-M-nitrobenzohydroxamic acid

Base Information

• Chemical Name: N-P-(Chlorophenyl)-M-nitrobenzohydroxamic acid
• CAS No.: 36016-30-5
• Molecular Formula: C₁₃H₉ClN₂O₄
• Molecular Weight: 292.678
• DSSTox Substance ID: DTXSID00189586
• Nikkaji Number: J1.618.400D
• Wikidata: Q83061733

Synonyms:N-P-(CHLOROPHENYL)-M-NITROBENZOHYDROXAMIC ACID;36016-30-5;DTXSID00189586;N-p-chlorophenyl-m-nitrobenzohydroxamic;N-Hydroxy-N-(4-chlorophenyl)-3-nitrobenzamide

Chemical Property of N-P-(Chlorophenyl)-M-nitrobenzohydroxamic acid

Chemical Property:

• Vapor Pressure: 1.59E-10mmHg at 25°C
• Boiling Point: 492.7°Cat760mmHg
• Flash Point: 251.8°C
• Density: 1.527g/cm³
• XLogP3: 2.9
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 2
• Exact Mass: 292.0250845
• Heavy Atom Count: 20
• Complexity: 366

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC(=CC(=C1)[N+](=O)[O-])C(=O)N(C2=CC=C(C=C2)Cl)O

Technology Process of N-P-(Chlorophenyl)-M-nitrobenzohydroxamic acid

There total 1 articles about N-P-(Chlorophenyl)-M-nitrobenzohydroxamic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ N-(4-chlorophenyl)-3-nitrobenzohydroxamic acid (36016-30-5)

Guidance literature:

DOI:10.1021/je60053a003

Reference yield:

N-(4-chlorophenyl)-3-nitrobenzohydroxamic acid (36016-30-5) + lanthanum(III) ion → La(3+)*3O2NC6H4C(O)N(O)C6H4Cl(1-)

Guidance literature:

With ammonia; In 1,4-dioxane; water; dropwise addn. of ligand in dioxane to warm (60°C) aq. soln. of rare earth salt (mixing); pptn. by aq. ammonia at pH range 6.2-7.0; 20-30 min digestion on water bath; centrifugation; washing (hot water and 20% aq. dioxane); drying at 110°C;

Reference yield:

N-(4-chlorophenyl)-3-nitrobenzohydroxamic acid (36016-30-5) + neodymium(III) → Nd(3+)*3O2NC6H4C(O)N(O)C6H4Cl(1-)

Guidance literature:

With ammonia; In 1,4-dioxane; water; dropwise addn. of ligand in dioxane to warm (60°C) aq. soln. of rare earth salt (mixing); pptn. by aq. ammonia at pH range 8.7-9.3; 20-30 min digestion on water bath; centrifugation; washing (hot water and 20% aq. dioxane); drying at 110°C;

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