Phosphonic acid, (cyclohexylmethyl)-, diethyl ester

Base Information

Chemical Name:Phosphonic acid, (cyclohexylmethyl)-, diethyl ester
CAS No.:63909-49-9
Molecular Formula:C11H23O3P
Molecular Weight:234.276
Hs Code.:
DSSTox Substance ID:DTXSID50440033
Nikkaji Number:J602.490D

Synonyms:63909-49-9;Phosphonic acid, (cyclohexylmethyl)-, diethyl ester;DTXSID50440033;(Cyclohexylmethyl)phosphonic acid diethyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Phosphonic acid, (cyclohexylmethyl)-, diethyl ester

Chemical Property:

XLogP3:2.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:6
Exact Mass:234.13848159
Heavy Atom Count:15
Complexity:202

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCOP(=O)(CC1CCCCC1)OCC

Technology Process of Phosphonic acid, (cyclohexylmethyl)-, diethyl ester

There total 5 articles about Phosphonic acid, (cyclohexylmethyl)-, diethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: Diethyl (chlorocyclohexylidenemethyl)phosphonate

: 63909-49-9
O,O-diethyl (cyclohexylmethyl)phosphonate

Guidance literature:: With hydrogen; sodium acetate; palladium on activated charcoal; In ethanol; for 17h; under 1810.02 Torr;
DOI:10.1021/jo00095a033

Reference yield: 82.0%

: 5707-06-2
O,O-diethyl Se-phenyl phosphoroselenoate

: 1192-37-6
methylenecyclohexane

: 63909-49-9
O,O-diethyl (cyclohexylmethyl)phosphonate

Guidance literature:: With 2,2'-azobis(isobutyronitrile); tris-(trimethylsilyl)silane; In benzene; for 3h; Heating;
DOI:10.1021/jo0348064

Reference yield:

: 866-23-9
diethyl (trichloromethyl)phosphonate

: 63909-49-9
O,O-diethyl (cyclohexylmethyl)phosphonate

Guidance literature:: Multi-step reaction with 2 steps

1: 59 percent / n-BuLi / tetrahydrofuran / 1.) -70 deg C, 1 h, 2.) r.t., 18 h

2: 90 percent / H₂, sodium acetate / 10percent Pd/C / ethanol / 17 h / 1810.02 Torr

With n-butyllithium; hydrogen; sodium acetate; palladium on activated charcoal; In tetrahydrofuran; ethanol;
DOI:10.1021/jo00095a033