4-Ethenyl-2-methyl-1-nitrobenzene

Base Information

Chemical Name:4-Ethenyl-2-methyl-1-nitrobenzene
CAS No.:63914-62-5
Molecular Formula:C9H9NO2
Molecular Weight:163.176
Hs Code.:2904209090
DSSTox Substance ID:DTXSID20493551
Wikidata:Q82340313

Synonyms:63914-62-5;4-Ethenyl-2-methyl-1-nitrobenzene;2-Methyl-1-nitro-4-vinylbenzene;SCHEMBL5458282;DTXSID20493551;OXLAWCNUPWRIRK-UHFFFAOYSA-N;2-methyl-1-nitro-4-vinyl-benzene;EN300-1851781

Suppliers and Price of 4-Ethenyl-2-methyl-1-nitrobenzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 4-Ethenyl-2-methyl-1-nitrobenzene

Chemical Property:

PSA：45.82000
LogP:3.06940
XLogP3:2.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:163.063328530
Heavy Atom Count:12
Complexity:186

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=C(C=CC(=C1)C=C)[N+](=O)[O-]

Technology Process of 4-Ethenyl-2-methyl-1-nitrobenzene

There total 1 articles about 4-Ethenyl-2-methyl-1-nitrobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 52415-00-6
4-iodo-2-methyl-1-nitro-benzene

: potassium vinyltrifluoroborate

: 63914-62-5
2-methyl-1-nitro-4-vinyl-benzene

Guidance literature:: With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium carbonate; In 1,4-dioxane; water; at 90 ℃; for 16h; Inert atmosphere;

Reference yield: 49.0%

: 63914-62-5
2-methyl-1-nitro-4-vinyl-benzene

: 2-(3-methyl-4-nitro-phenyl)-ethanol

Guidance literature:: 2-methyl-1-nitro-4-vinyl-benzene; With dimethylsulfide borane complex; In tetrahydrofuran; at 0 - 20 ℃; for 4h; Inert atmosphere;

With dihydrogen peroxide; sodium hydroxide; In water; at 20 ℃; for 14h;

Reference yield:

: 63914-62-5
2-methyl-1-nitro-4-vinyl-benzene

: C₉H₁₁NO

Guidance literature:: With water; ammonium chloride; zinc; In tetrahydrofuran; at 0 ℃; for 3h; Inert atmosphere;
DOI:10.1021/acs.orglett.0c01009