6-(dimethylamino)-N,N-dimethyl-2,4-dithioxo-2H-1,3,5-thiadiazine-3(4H)-carbothioamide

Base Information

• Chemical Name: 6-(dimethylamino)-N,N-dimethyl-2,4-dithioxo-2H-1,3,5-thiadiazine-3(4H)-carbothioamide
• CAS No.: 16011-82-8
• Molecular Formula: C₈H₁₂N₄S₄
• Molecular Weight: 292.474
• Mol file: 16011-82-8.mol

Synonyms:2H-1,3,5-Thiadiazine-3(4H)-carboxamide,6-(dimethylamino)-N,N-dimethylthio-2,4-dithioxo- (8CI); NSC 330171

Chemical Property of 6-(dimethylamino)-N,N-dimethyl-2,4-dithioxo-2H-1,3,5-thiadiazine-3(4H)-carbothioamide

Chemical Property:

• Vapor Pressure: 3.32E-05mmHg at 25°C
• Boiling Point: 354.6°Cat760mmHg
• Flash Point: 168.2°C
• Density: 1.41g/cm³

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 6-(dimethylamino)-N,N-dimethyl-2,4-dithioxo-2H-1,3,5-thiadiazine-3(4H)-carbothioamide

There total 2 articles about 6-(dimethylamino)-N,N-dimethyl-2,4-dithioxo-2H-1,3,5-thiadiazine-3(4H)-carbothioamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-dimethylamino-1,2,4-dithiazole-5-thione (30013-32-2) → 3-(N,N-Dimethyl-thiocarbamoyl)-6-dimethylamino-2,3-dihydro-4H-1,3,5-thiadiazin-2,4-dithion (16011-82-8)

Guidance literature:

for 48h; Ambient temperature;

DOI:10.1021/jo01269a078

Reference yield:

sodium thiocyanide (540-72-7) + N,N-Dimethylthiocarbamoyl chloride (16420-13-6) → 3-(N,N-Dimethyl-thiocarbamoyl)-6-dimethylamino-2,3-dihydro-4H-1,3,5-thiadiazin-2,4-dithion (16011-82-8)

Guidance literature:

Multistep reaction; (i) ,(ii) AcOEt;

DOI:10.1016/S0040-4039(00)76154-5

upstream raw materials:

3-dimethylamino-1,2,4-dithiazole-5-thione

sodium thiocyanide

N,N-Dimethylthiocarbamoyl chloride

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