4-(BROMOMETHYL)-5-METHYL-2-PHENYL-2H-1,2,3-TRIAZOLE

Base Information

• Chemical Name: 4-(BROMOMETHYL)-5-METHYL-2-PHENYL-2H-1,2,3-TRIAZOLE
• CAS No.: 13322-02-6
• Molecular Formula: C10H10 Br N3
• Molecular Weight: 252.113
• Hs Code.: 2933990090
• Mol file: 13322-02-6.mol

Synonyms:4-Bromomethyl-5-methyl-2-phenyl-2H-[1,2,3]triazole;NSC 362341

Chemical Property of 4-(BROMOMETHYL)-5-METHYL-2-PHENYL-2H-1,2,3-TRIAZOLE

Chemical Property:

• Vapor Pressure: 6.31E-06mmHg at 25°C
• Melting Point: 72℃
• Boiling Point: 378.4°Cat760mmHg
• PKA: 0.38±0.20(Predicted)
• Flash Point: 182.6°C
• PSA: 30.71000
• Density: 1.49g/cm³
• LogP: 2.47060

Purity/Quality:

97% ^*data from raw suppliers

4-(BROMOMETHYL)-5-METHYL-2-PHENYL-2H-1,2,3-TRIAZOLE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s): R34:Causes burns.
• Hazard Codes: C:Corrosive
• Statements: R34:Causes burns.
• Safety Statements: S26:In case of contact with eyes, rinse immediately with plenty of water and seek medical advice.; S36/37/39:Wear suitabl

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-(BROMOMETHYL)-5-METHYL-2-PHENYL-2H-1,2,3-TRIAZOLE

There total 2 articles about 4-(BROMOMETHYL)-5-METHYL-2-PHENYL-2H-1,2,3-TRIAZOLE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(5-methyl-2-phenyl-2H-1,2,3-triazol-4-yl) methanol (13322-19-5) → 4-(bromomethyl)-5-methyl-2-phenyl-2H-1,2,3-triazole (13322-02-6)

Guidance literature:

With phosphorus tribromide; In dichloromethane; at 0 ℃; for 1h;

Reference yield:

→ 4-(bromomethyl)-5-methyl-2-phenyl-2H-1,2,3-triazole (13322-02-6)

Guidance literature:

4,5-Dimethyl-2-phenyl-2H-1,2,3-triazol, N-Bromsuccinimid+Dibenzoylperoxyd ;

Reference yield: 95.0%

sodium cyanide (143-33-9,25596-52-5) + 4-(bromomethyl)-5-methyl-2-phenyl-2H-1,2,3-triazole (13322-02-6) → (5-methyl-2-phenyl-2H-[1,2,3]triazol-4-yl)-acetonitrile (13322-20-8)

Guidance literature:

In N,N-dimethyl-formamide; at 23 - 60 ℃; for 17h;

upstream raw materials:

(5-methyl-2-phenyl-2H-1,2,3-triazol-4-yl) methanol

Downstream raw materials:

(5-methyl-2-phenyl-2H-[1,2,3]triazol-4-yl)-acetonitrile

2-[4-[[tert-butoxycarbamoylmethyl-(5-methyl-2-phenyl-2H-[1,2,3]triazol-4-ylmethyl)amino]methyl]-2,6-dimethylphenoxy]-2-methylpropionic acid ethyl ester

N-(4-fluorophenyl)-6-((5-methyl-2-phenyl-2H-1,2,3-triazol-4-yl)methylthio)nicotinamide

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