2,6-DINITRO-4-(ACETYL)AMINOTOLUENE

Base Information

• Chemical Name: 2,6-DINITRO-4-(ACETYL)AMINOTOLUENE
• CAS No.: 7142-91-8
• Molecular Formula: C9H9 N3 O5
• Molecular Weight: 239.188
• Mol file: 7142-91-8.mol

Synonyms:p-Acetotoluidide,3',5'-dinitro- (6CI,8CI); NSC 56668

Chemical Property of 2,6-DINITRO-4-(ACETYL)AMINOTOLUENE

Chemical Property:

• Vapor Pressure: 8.78E-07mmHg at 25°C
• Boiling Point: 405.4°C at 760 mmHg
• Flash Point: 199°C
• PSA: 120.74000
• Density: 1.472g/cm³
• LogP: 2.88920

Purity/Quality:

2,6-DINITRO-4-(ACETYL)AMINOTOLUENE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2,6-DINITRO-4-(ACETYL)AMINOTOLUENE

There total 2 articles about 2,6-DINITRO-4-(ACETYL)AMINOTOLUENE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,4,6-Trinitrotoluene (118-96-7) → 4-acetylamino-2,6-dinitrotoluene (7142-91-8)

Guidance literature:

Multi-step reaction with 2 steps

1: dioxane; sulfur hydrogen; water; ammonia

With 1,4-dioxane; ammonia; water; sulfur;

DOI:10.1039/jr9480001275

Reference yield:

4-Amino-2,6-dinitrotoluene (19406-51-0,153919-64-3) → 4-acetylamino-2,6-dinitrotoluene (7142-91-8)

Guidance literature:

DOI:10.1039/jr9480001275

Reference yield:

4-acetylamino-2,6-dinitrotoluene (7142-91-8) → 4-Methyl-3-nitroanilin (119-32-4)

Guidance literature:

Multi-step reaction with 3 steps

1: aqueous ethanol; 4>2S

2: H₃PO₄; aqueous NaNO₂

3: aqueous HCl / Hydrogenation

With hydrogenchloride; diammonium sulfide; ethanol; phosphoric acid; sodium nitrite;

DOI:10.1021/ja01165a034

upstream raw materials:

4-Amino-2,6-dinitrotoluene

2,4,6-Trinitrotoluene

Downstream raw materials:

4-N-acetylamino-2-amino-6-nitrotoluene

4-acetylamino-2-nitrotoluene

4-Methyl-3-nitroanilin