pentacopper; azanide; 4-(3,4,5,6-tetrahydro-2H-pyridin-4-yl)pyridine; 4-(3,4,5,6-tetrahydro-2H-pyridin-4-yl)-6H-pyridine; 4-(3,4,5,6-tetrahydro-2H-pyridin-4-yl)-3,4,5,6-tetrahydro-2H-pyridine; tetrahydrate

Base Information

• Chemical Name: pentacopper; azanide; 4-(3,4,5,6-tetrahydro-2H-pyridin-4-yl)pyridine; 4-(3,4,5,6-tetrahydro-2H-pyridin-4-yl)-6H-pyridine; 4-(3,4,5,6-tetrahydro-2H-pyridin-4-yl)-3,4,5,6-tetrahydro-2H-pyridine; tetrahydrate
• CAS No.: 7225-55-0
• Molecular Formula: C₉H₁₈O₆
• Molecular Weight: 222.238

Synonyms:

Chemical Property of pentacopper; azanide; 4-(3,4,5,6-tetrahydro-2H-pyridin-4-yl)pyridine; 4-(3,4,5,6-tetrahydro-2H-pyridin-4-yl)-6H-pyridine; 4-(3,4,5,6-tetrahydro-2H-pyridin-4-yl)-3,4,5,6-tetrahydro-2H-pyridine; tetrahydrate

Chemical Property:

• Boiling Point: 278.6°Cat760mmHg
• Flash Point: 151.5°C
• Density: g/cm³

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of pentacopper; azanide; 4-(3,4,5,6-tetrahydro-2H-pyridin-4-yl)pyridine; 4-(3,4,5,6-tetrahydro-2H-pyridin-4-yl)-6H-pyridine; 4-(3,4,5,6-tetrahydro-2H-pyridin-4-yl)-3,4,5,6-tetrahydro-2H-pyridine; tetrahydrate

There total 8 articles about pentacopper; azanide; 4-(3,4,5,6-tetrahydro-2H-pyridin-4-yl)pyridine; 4-(3,4,5,6-tetrahydro-2H-pyridin-4-yl)-6H-pyridine; 4-(3,4,5,6-tetrahydro-2H-pyridin-4-yl)-3,4,5,6-tetrahydro-2H-pyridine; tetrahydrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

diazomethane (186581-53-3,908094-01-9,334-88-3) + methyl-alpha-D-glucopyranoside (97-30-3) → methyl α-D-glucopyranoside 3-methyl ether (5149-37-1) + methyl 2,3-di-O-methyl-α-D-glucopyranoside (10227-29-9,14048-30-7,22323-70-2,22323-71-3,23397-51-5,27299-05-4,31085-63-9,66808-29-5,66808-32-0,74560-65-9,91176-73-7,94992-18-4,110416-07-4) + methyl-2,4-di-O-methyl-α-D-glucopyranoside (28954-20-3) + methyl 2,6-di-O-methyl-α-D-glucopyranoside (7225-55-0,22323-69-9,23392-38-3,23397-50-4,59830-21-6,65877-27-2,65877-28-3)

Guidance literature:

With antimony(III) chloride; In methanol; dichloromethane; at 20 ℃; for 2h; Further byproducts given;

DOI:10.1016/S0008-6215(99)00044-0

Reference yield:

diazomethane (186581-53-3,908094-01-9,334-88-3) + methyl-alpha-D-glucopyranoside (97-30-3) → Methyl-2,4,6-tri-O-methyl-α-D-glucopyranosid (35939-72-1) + methyl 2,3-di-O-methyl-α-D-glucopyranoside (10227-29-9,14048-30-7,22323-70-2,22323-71-3,23397-51-5,27299-05-4,31085-63-9,66808-29-5,66808-32-0,74560-65-9,91176-73-7,94992-18-4,110416-07-4) + methyl-2,4-di-O-methyl-α-D-glucopyranoside (28954-20-3) + methyl 2,6-di-O-methyl-α-D-glucopyranoside (7225-55-0,22323-69-9,23392-38-3,23397-50-4,59830-21-6,65877-27-2,65877-28-3)

Guidance literature:

With water; In diethyl ether; at 25 ℃; for 48h; Further byproducts given. Title compound not separated from byproducts;

DOI:10.1016/0008-6215(87)80024-1

Reference yield:

diazomethane (186581-53-3,908094-01-9,334-88-3) + methyl-alpha-D-glucopyranoside (97-30-3) → methyl 3,4-di-O-methyl-α-D-glucopyranoside (23262-69-3) + Methyl-2,4,6-tri-O-methyl-α-D-glucopyranosid (35939-72-1) + methyl 2,3-di-O-methyl-α-D-glucopyranoside (10227-29-9,14048-30-7,22323-70-2,22323-71-3,23397-51-5,27299-05-4,31085-63-9,66808-29-5,66808-32-0,74560-65-9,91176-73-7,94992-18-4,110416-07-4) + methyl 2,6-di-O-methyl-α-D-glucopyranoside (7225-55-0,22323-69-9,23392-38-3,23397-50-4,59830-21-6,65877-27-2,65877-28-3)

Guidance literature:

With water; In diethyl ether; at 25 ℃; for 48h; Further byproducts given. Title compound not separated from byproducts;

DOI:10.1016/0008-6215(87)80024-1

upstream raw materials:

diazomethane

methyl-alpha-D-glucopyranoside

(2R,3S,4S,5S,6S)-2-(hydroxymethyl)-6-methoxytetrahydro-2H-pyran-3,4,5-triol

dimethyl sulfate

Downstream raw materials:

Methyl-3-O-benzyl-4-O-(2,3-di-O-benzyl-6-desoxy-4-O-methyl-α-D-galactopyranosyl)-2,6-di-O-methyl-α-D-mannopyranosid

C₃₇H₄₈O₁₀

Methyl-4-O-benzyl-3-O-(2,3-di-O-acetyl-6-desoxy-4-O-methyl-β-D-galactopyranosyl)-2,6-di-O-methyl-α-D-mannopyranosid

Methyl-3-O-benzyl-4-O-(2,3-di-O-acetyl-6-desoxy-4-O-methyl-β-D-galactopyranosyl)-2,6-di-O-methyl-α-D-mannopyranosid

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