10-bromo-2-methyl-11b-phenyl-2,3,7,11b-tetrahydro[1,3]oxazolo[3,2-d][1,4]benzodiazepin-6(5H)-one

Base Information

Chemical Name:10-bromo-2-methyl-11b-phenyl-2,3,7,11b-tetrahydro[1,3]oxazolo[3,2-d][1,4]benzodiazepin-6(5H)-one
CAS No.:24143-24-6
Molecular Formula:C₁₈H₁₇BrN₂O₂
Molecular Weight:373.249
Hs Code.:
Mol file:24143-24-6.mol

Synonyms:10-bromo-2-methyl-11b-phenyl-2,3,7,11b-tetrahydro[1,3]oxazolo[3,2-d][1,4]benzodiazepin-6(5h)-one;10-bromo-2-methyl-11b-phenyl-2,3,7,11b-hexahydro-benzo[f]oxazolo[3,2-e][1,4]diazepin-6-one;2,3,7,11b-Tetrahydro-10-bromo-2-methyl-11b-phenyloxazolo(3,2-d)(1,4)benzodiazepin-6(5H)-one;Oxazolo(3,2-d)(1,4)benzodiazepin-6(5H)-one,2,3,7,11b-tetrahydro-10-bromo-2-methyl-11b-phenyl;

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 10-bromo-2-methyl-11b-phenyl-2,3,7,11b-tetrahydro[1,3]oxazolo[3,2-d][1,4]benzodiazepin-6(5H)-one

Chemical Property:

Vapor Pressure:2.19E-10mmHg at 25°C
Boiling Point:506.6°Cat760mmHg
Flash Point:260.2°C
PSA：45.06000
Density:1.54g/cm³
LogP:3.34600

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 10-bromo-2-methyl-11b-phenyl-2,3,7,11b-tetrahydro[1,3]oxazolo[3,2-d][1,4]benzodiazepin-6(5H)-one

There total 3 articles about 10-bromo-2-methyl-11b-phenyl-2,3,7,11b-tetrahydro[1,3]oxazolo[3,2-d][1,4]benzodiazepin-6(5H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 24111-62-4
N-(2-hydroxy-propyl)-glycine 2-benzoyl-4-bromo-anilide

: 24143-24-6,35100-02-8
10-bromo-2t-methyl-11b-phenyl-(11br)-2,3,7,11b-hexahydro-benzo[f]oxazolo[3,2-e][1,4]diazepin-6-one

Guidance literature:: With acetic acid; In ethanol; Heating;
DOI:10.1021/jm00288a015

Reference yield:

: 7-Bromo-4-(2-hydroxy-propyl)-2-oxo-5-phenyl-2,3-dihydro-1H-benzo[e][1,4]diazepin-4-ium

: 24143-24-6
10-bromo-2-methyl-11b-phenyl-2,3,7,11b-hexahydro-benzo[f]oxazolo[3,2-e][1,4]diazepin-6-one

Guidance literature:: With borate buffer (pH=8-10.5); In ethanol; water; Equilibrium constant; Mechanism; variation of pH and buffers.;
DOI:10.1248/cpb.30.3810