3-(β-nitro-β-methylvinyl)indole

Base Information

Chemical Name:3-(β-nitro-β-methylvinyl)indole
CAS No.:64252-02-4
Molecular Formula:C11H10N2O2
Molecular Weight:202.213
Hs Code.:
Mol file:64252-02-4.mol

Synonyms:3-(2-nitro-propenyl)-1H-indole;3-(2-nitropropenyl)-1H-indole;3-(2-nitro-propenyl)-indole;(E)-3-(2-nitroprop-1-enyl)-1H-indole;3-(2-Nitro-propenyl)-indol;1-(3-indolyl)-2-nitropropene;

Suppliers and Price of 3-(β-nitro-β-methylvinyl)indole

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of 3-(β-nitro-β-methylvinyl)indole

Chemical Property:

Melting Point:194-196 °C
Boiling Point:402.2±20.0 °C(Predicted)
PKA:16.09±0.30(Predicted)
PSA：61.61000
Density:1.300±0.06 g/cm3(Predicted)
LogP:3.32860

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 3-(β-nitro-β-methylvinyl)indole

There total 3 articles about 3-(β-nitro-β-methylvinyl)indole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 487-89-8,1228547-52-1
Indole-3-carboxaldehyde

: 79-24-3
Nitroethane

: 64252-02-4
3-(β-nitro-β-methylvinyl)indole

Guidance literature:: With ammonium acetate; for 6h; Reflux;
DOI:10.1039/c0ob00800a

Reference yield: 84.2%

: 64252-02-4
3-(β-nitro-β-methylvinyl)indole

Guidance literature:: With cyclohexylamine; for 0.333333h; Cooling with ice;

With acetic acid; at 70 ℃; for 2h;

Reference yield:

: 83-34-1
3-Methylindole

: 64252-02-4
3-(β-nitro-β-methylvinyl)indole

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) 2,3-dichloro-5,6-dicyan-p-benzoquinone; 2.) potassium carbonate / 1.) tetrahydrofuran, water, room temperature, 10 h; 2.) 1 h

2: 75 percent / ammonium acetate / 2 h / 120 - 130 °C

With potassium carbonate; 2,3-dicyano-5,6-dichloro-p-benzoquinone; ammonium acetate;
DOI:10.1016/0223-5234(89)90161-X