10-(4-bromophenyl)-5H-phenarsazinine

Base Information

• Chemical Name: 10-(4-bromophenyl)-5H-phenarsazinine
• CAS No.: 64268-49-1
• Molecular Formula: C₁₈H₁₃AsBrN
• Molecular Weight: 398.134
• DSSTox Substance ID: DTXSID00548619
• Wikidata: Q82427375

Synonyms:64268-49-1;DTXSID00548619;10-(4-Bromophenyl)-5,10-dihydrophenazarsinine

Chemical Property of 10-(4-bromophenyl)-5H-phenarsazinine

Chemical Property:

• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 1
• Exact Mass: 396.94473
• Heavy Atom Count: 21
• Complexity: 333

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C2C(=C1)NC3=CC=CC=C3[As]2C4=CC=C(C=C4)Br

Technology Process of 10-(4-bromophenyl)-5H-phenarsazinine

There total 1 articles about 10-(4-bromophenyl)-5H-phenarsazinine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

adamsite (578-94-9) + (4-bromophenyl)magnesium bromide (18620-02-5) → 10-(p-bromophenyl)-5,10-dihydrophenarsazine (64268-49-1)

Guidance literature:

In tetrahydrofuran;

Reference yield:

10-(p-bromophenyl)-5,10-dihydrophenarsazine (64268-49-1) → 10-(4-bromo-phenyl)-5,10-dihydro-phenarsazine 10-oxide (64268-58-2)

Guidance literature:

With dihydrogen peroxide; In acetone;

Reference yield:

dimethyl sulfate (77-78-1) + 10-(p-bromophenyl)-5,10-dihydrophenarsazine (64268-49-1) → 10-(p-bromophenyl)-5,10-dihydro-5-methylphenarsazine

Guidance literature:

With ethylmagnesium bromide; Yield given. Multistep reaction; 1.) THF, 1 h; 2.) THF, 1 h;

upstream raw materials:

adamsite

(4-bromophenyl)magnesium bromide

Downstream raw materials:

10-(4-bromo-phenyl)-5,10-dihydro-phenarsazine 10-oxide

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