1H-Pyrrole-3-propanoic acid, 2-[(1,1-dimethylethoxy)carbonyl]-5-[[3-ethyl-4-methyl-5-[(phenylmethoxy) carbonyl]-1H-pyrrol-2-yl]methyl]-4-methyl-, methyl ester

Base Information

Chemical Name:1H-Pyrrole-3-propanoic acid, 2-[(1,1-dimethylethoxy)carbonyl]-5-[[3-ethyl-4-methyl-5-[(phenylmethoxy) carbonyl]-1H-pyrrol-2-yl]methyl]-4-methyl-, methyl ester
CAS No.:64271-04-1
Molecular Formula:C30H38N2O6
Molecular Weight:522.642
Hs Code.:

1H-Pyrrole-3-propanoic acid,
2-[(1,1-dimethylethoxy)carbonyl]-5-[[3-ethyl-4-methyl-5-[(phenylmethoxy)
carbonyl]-1H-pyrrol-2-yl]methyl]-4-methyl-, methyl ester

Synonyms:

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Chemical Property of 1H-Pyrrole-3-propanoic acid, 2-[(1,1-dimethylethoxy)carbonyl]-5-[[3-ethyl-4-methyl-5-[(phenylmethoxy) carbonyl]-1H-pyrrol-2-yl]methyl]-4-methyl-, methyl ester

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MSDS Files:: SDS file from LookChem

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Technology Process of 1H-Pyrrole-3-propanoic acid, 2-[(1,1-dimethylethoxy)carbonyl]-5-[[3-ethyl-4-methyl-5-[(phenylmethoxy) carbonyl]-1H-pyrrol-2-yl]methyl]-4-methyl-, methyl ester

There total 4 articles about 1H-Pyrrole-3-propanoic acid, 2-[(1,1-dimethylethoxy)carbonyl]-5-[[3-ethyl-4-methyl-5-[(phenylmethoxy) carbonyl]-1H-pyrrol-2-yl]methyl]-4-methyl-, methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 3750-36-5
benzyl 5-(acetoxymethyl)-4-ethyl-3-methyl-1H-pyrrole-2-carboxylate

: 42419-19-2
tert-butyl 3-(2-methoxycarbonylethyl)-4-methylpyrrole-2-carboxylate

: 64271-04-1
tert-butyl 5'-(benzyloxycarbonyl)-3'-ethyl-4-(2-methoxycarbonylethyl)-3,4'-dimethyl-2,2'-dipyrrylmethane-5-carboxylate

Guidance literature:: With Montmorillonite clay K-10; In chloroform; for 24h;
DOI:10.1021/jo981473f

Reference yield: 18.0%

: 31837-47-5
4-(2'-methoxycarbonylethyl)-3-methyl-5-t-butoxycarbonylpyrrole-2-carboxylic acid

: 52459-91-3
1-(5-benzyloxycarbonyl-3-ethyl-4-methyl-2-pyrrolylmethyl)pyridinium bromide

: 64271-04-1
tert-butyl 5'-(benzyloxycarbonyl)-3'-ethyl-4-(2-methoxycarbonylethyl)-3,4'-dimethyl-2,2'-dipyrrylmethane-5-carboxylate

Guidance literature:: With lithium methanolate; In formamide; at 100 ℃; for 24h;
DOI:10.1039/P19870000287

Reference yield:

: 31837-48-6
t-butyl 5-iodo-3-(2-methoxycarbonylethyl)-4-methylpyrrole-2-carboxylate

: 64271-04-1
tert-butyl 5'-(benzyloxycarbonyl)-3'-ethyl-4-(2-methoxycarbonylethyl)-3,4'-dimethyl-2,2'-dipyrrylmethane-5-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / H₂, anhydr. sodium acetate / platinum oxide / methanol / 20 °C / 760 Torr

2: 60 percent / toluene-p-sulphonic acid / acetic acid / 10 h / 40 °C

With hydrogen; sodium acetate; toluene-4-sulfonic acid; platinum(IV) oxide; In methanol; acetic acid;
DOI:10.1039/P19870000287