4-(Triisopropylsilyloxy)phenyl Boronic Acid

Base Information

Chemical Name:4-(Triisopropylsilyloxy)phenyl Boronic Acid
CAS No.:643090-93-1
Molecular Formula:C15H27BO3Si
Molecular Weight:294.274
Hs Code.:
Mol file:643090-93-1.mol

Synonyms:4-(Triisopropylsilyloxy)phenyl Boronic Acid;

Suppliers and Price of 4-(Triisopropylsilyloxy)phenyl Boronic Acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
4-(Triisopropylsilyloxy)phenylBoronicAcid
1g
$ 1230.00

American Custom Chemicals Corporation
4-(TRIISOPROPYLSILYLOXY)PHENYL BORONIC ACID 95.00%
1G
$ 1871.10

American Custom Chemicals Corporation
4-(TRIISOPROPYLSILYLOXY)PHENYL BORONIC ACID 95.00%
100MG
$ 739.20

Total 2 raw suppliers

Chemical Property of 4-(Triisopropylsilyloxy)phenyl Boronic Acid

Chemical Property:

PSA：49.69000
LogP:2.92070
Solubility.:Chloroform, Dichloromethane, Methanol

Purity/Quality:

97% ^*data from raw suppliers

4-(Triisopropylsilyloxy)phenylBoronicAcid ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Uses Intermediate in the preparation of Thyroxin derivatives.

Technology Process of 4-(Triisopropylsilyloxy)phenyl Boronic Acid

There total 12 articles about 4-(Triisopropylsilyloxy)phenyl Boronic Acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 5419-55-6
Triisopropyl borate

: 180577-83-7
1-iodo-4-[[tris(1-methylethyl)silyl]oxy]benzene

: 643090-93-1
(4-((triisopropylsilyl)oxy)phenyl)boronic acid

Guidance literature:: 1-iodo-4-[[tris(1-methylethyl)silyl]oxy]benzene; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.5h;

Triisopropyl borate; In tetrahydrofuran; hexane; at -78 ℃; for 80h;

With hydrogenchloride; In tetrahydrofuran; hexane;

Reference yield: 96.0%

: 5419-55-6
Triisopropyl borate

: (4-(2-iodoethyl)phenoxy)triisopropylsilane

: 643090-93-1
(4-((triisopropylsilyl)oxy)phenyl)boronic acid

Guidance literature:: (4-(2-iodoethyl)phenoxy)triisopropylsilane; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.5h;

Triisopropyl borate; In tetrahydrofuran; hexane; at -78 - 20 ℃; for 1.33333h;
DOI:10.1021/acs.jmedchem.6b00177

Reference yield: 88.0%

: 193966-77-7
4-bromo-1-(triisopropylsilyloxy)benzene

: 643090-93-1
(4-((triisopropylsilyl)oxy)phenyl)boronic acid

Guidance literature:: 4-bromo-1-(triisopropylsilyloxy)benzene; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.5h;

With Triisopropyl borate; In tetrahydrofuran; hexane; at 20 ℃; for 1h;

With hydrogenchloride; In tetrahydrofuran; hexane; at 20 ℃; Further stages.;
DOI:10.1016/j.bmc.2007.10.040