1,3-Dimethyl-N-phenyl-1H-pyrazole-4-carboxamide

Base Information

Chemical Name:1,3-Dimethyl-N-phenyl-1H-pyrazole-4-carboxamide
CAS No.:64429-34-1
Molecular Formula:C₁₂H₁₃N₃O
Molecular Weight:215.255
Hs Code.:
DSSTox Substance ID:DTXSID10515756
Wikidata:Q82376816

Synonyms:64429-34-1;SCHEMBL11541530;DTXSID10515756;WZBRFGKKALNVLH-UHFFFAOYSA-N;1,3-dimethyl-N-phenyl-4-pyrazolecarboxamide;1,3-Dimethyl-N-phenyl-1H-pyrazole-4-carboxamide

Suppliers and Price of 1,3-Dimethyl-N-phenyl-1H-pyrazole-4-carboxamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 1,3-Dimethyl-N-phenyl-1H-pyrazole-4-carboxamide

Chemical Property:

XLogP3:1.5
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:215.105862047
Heavy Atom Count:16
Complexity:251

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=NN(C=C1C(=O)NC2=CC=CC=C2)C

Technology Process of 1,3-Dimethyl-N-phenyl-1H-pyrazole-4-carboxamide

There total 3 articles about 1,3-Dimethyl-N-phenyl-1H-pyrazole-4-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2749-59-9
1,3-dimethyl-5-pyrazolone

: 64429-34-1
1,3-dimethyl-N-phenylpyrazole-4-carboxamide

Guidance literature:: Multi-step reaction with 3 steps

1: 72 percent / triethylamine / benzene

2: 70 percent / phosphoryl chloride, diethylaniline / 0.5 h / Heating

3: 91 percent / H₂, anhydrous sodium acetate / 5percent Pd/C / ethanol / 1520 Torr / Ambient temperature

With hydrogen; sodium acetate; triethylamine; N,N-diethylaniline; trichlorophosphate; palladium on activated charcoal; In ethanol; benzene;
DOI:10.1071/CH9830135

Reference yield:

: 64429-35-2
1,3-dimethyl-5-oxo-N-phenyl-4,5-dihydro-1H-pyrazole-4-carboxamide

: 64429-34-1
1,3-dimethyl-N-phenylpyrazole-4-carboxamide

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / phosphoryl chloride, diethylaniline / 0.5 h / Heating

2: 91 percent / H₂, anhydrous sodium acetate / 5percent Pd/C / ethanol / 1520 Torr / Ambient temperature

With hydrogen; sodium acetate; N,N-diethylaniline; trichlorophosphate; palladium on activated charcoal; In ethanol;
DOI:10.1071/CH9830135