Benzoic acid, 2-formyl-3-hydroxy-5-methoxy-6-methyl-, 4-[[(1R)-2-methoxy-2-oxo-1-[[(triphenylmethyl)thio]methyl]ethyl]amino]-4- oxobutyl ester

Base Information

• Chemical Name: Benzoic acid, 2-formyl-3-hydroxy-5-methoxy-6-methyl-, 4-[[(1R)-2-methoxy-2-oxo-1-[[(triphenylmethyl)thio]methyl]ethyl]amino]-4- oxobutyl ester
• CAS No.: 647026-22-0
• Molecular Formula: C₃₇H₃₇NO₈S
• Molecular Weight: 655.769

Synonyms:

Chemical Property of Benzoic acid, 2-formyl-3-hydroxy-5-methoxy-6-methyl-, 4-[[(1R)-2-methoxy-2-oxo-1-[[(triphenylmethyl)thio]methyl]ethyl]amino]-4- oxobutyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Benzoic acid, 2-formyl-3-hydroxy-5-methoxy-6-methyl-, 4-[[(1R)-2-methoxy-2-oxo-1-[[(triphenylmethyl)thio]methyl]ethyl]amino]-4- oxobutyl ester

There total 1 articles about Benzoic acid, 2-formyl-3-hydroxy-5-methoxy-6-methyl-, 4-[[(1R)-2-methoxy-2-oxo-1-[[(triphenylmethyl)thio]methyl]ethyl]amino]-4- oxobutyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(R)-2-(4-Bromo-butyrylamino)-3-tritylsulfanyl-propionic acid methyl ester (647026-17-3) + 2-formyl-3-hydroxy-5-methoxy-6-methyl-benzoic acid; compound with N,N,N',N'-tetramethyl-guanidine → 2-Formyl-3-hydroxy-5-methoxy-6-methyl-benzoic acid 3-((R)-1-methoxycarbonyl-2-tritylsulfanyl-ethylcarbamoyl)-propyl ester (647026-22-0) + 3-Hydroxy-5-methoxy-2-{[(E)-(R)-1-methoxycarbonyl-2-tritylsulfanyl-ethylimino]-methyl}-6-methyl-benzoic acid 3-((R)-1-methoxycarbonyl-2-tritylsulfanyl-ethylcarbamoyl)-propyl ester

Guidance literature:

In N,N-dimethyl-formamide; at 50 ℃; for 12h;

upstream raw materials:

(R)-2-(4-Bromo-butyrylamino)-3-tritylsulfanyl-propionic acid methyl ester

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