2,4,6-Octatrienedioic acid, 2,7-dimethyl-, diethyl ester, (E,E,E)-

Base Information

Chemical Name:2,4,6-Octatrienedioic acid, 2,7-dimethyl-, diethyl ester, (E,E,E)-
CAS No.:64768-01-0
Molecular Formula:C14H20O4
Molecular Weight:252.31
Hs Code.:

Synonyms:

Suppliers and Price of 2,4,6-Octatrienedioic acid, 2,7-dimethyl-, diethyl ester, (E,E,E)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2,4,6-Octatrienedioic acid, 2,7-dimethyl-, diethyl ester, (E,E,E)-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2,4,6-Octatrienedioic acid, 2,7-dimethyl-, diethyl ester, (E,E,E)-

There total 1 articles about 2,4,6-Octatrienedioic acid, 2,7-dimethyl-, diethyl ester, (E,E,E)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6111-99-5
ethyl diazoalaninate

: 64768-01-0
diethyl 2,7-dimethyl-2(E),4(E),6(E)-octatriene-1,8-dioate

Guidance literature:: Multi-step reaction with 2 steps

1: 2) iodine / 1) dirhodium tetraacetate / 1) 18 h, 2) CH₂Cl₂, RT, 6 h

2: 1) NaH / 1) THF, 10 min, RT, 2) THF, 12 h

With iodine; sodium hydride; dirhodium tetraacetate;
DOI:10.1021/jo00312a031

Reference yield:

: 64768-01-0
diethyl 2,7-dimethyl-2(E),4(E),6(E)-octatriene-1,8-dioate

: 27876-94-4
crocetin

Guidance literature:: Multi-step reaction with 5 steps

1: diisobutylaluminium hydride / hexane / 3 h / -78 - -20 °C / Inert atmosphere

2: manganese(IV) oxide / acetone / 0 - 20 °C

3: toluene / 6 h / 130 °C / Reflux

4: sodium hydroxide / water; methanol / Reflux

5: phosphoric acid

With manganese(IV) oxide; phosphoric acid; diisobutylaluminium hydride; sodium hydroxide; In methanol; hexane; water; acetone; toluene;
DOI:10.1021/acs.jafc.7b01668

Reference yield:

: 64768-01-0
diethyl 2,7-dimethyl-2(E),4(E),6(E)-octatriene-1,8-dioate

: 5056-17-7
(2E,4E,6E)-2,7-dimethyl-2,4,6-octatrienedial

Guidance literature:: Multi-step reaction with 2 steps

1: diisobutylaluminium hydride / hexane / 3 h / -78 - -20 °C / Inert atmosphere

2: manganese(IV) oxide / acetone / 0 - 20 °C

With manganese(IV) oxide; diisobutylaluminium hydride; In hexane; acetone;
DOI:10.1021/acs.jafc.7b01668