3,15-diacetylbenzoylaconine

Base Information

• Chemical Name: 3,15-diacetylbenzoylaconine
• CAS No.: 119347-27-2
• Molecular Formula: C₃₆H₄₉NO₁₂
• Molecular Weight: 687.785
• Mol file: 119347-27-2.mol

Synonyms:2H-12,3,6a-Ethanylylidene-7,9-methanonaphth[2,3-b]azocine,aconitane-3,8,13,14,15-pentol deriv.; 3,15-Diacetylbenzoylaconine;Picraconitine 3,15-diacetate; Polyschistine D 15-acetate

Chemical Property of 3,15-diacetylbenzoylaconine

Chemical Property:

• Vapor Pressure: 1.26E-21mmHg at 25°C
• Boiling Point: 717.8°Cat760mmHg
• Flash Point: 387.9°C
• PSA: 159.52000
• Density: 1.36g/cm³
• LogP: 1.15680

Purity/Quality:

99%min ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3,15-diacetylbenzoylaconine

There total 3 articles about 3,15-diacetylbenzoylaconine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

monoacetylaconitine (77181-26-1) → 3,15-diacetylbenzoylaconine (119347-27-2)

Guidance literature:

Multi-step reaction with 2 steps

1: 83 mg / water / dioxane / 1 h / Heating

2: pyridine / Ambient temperature

With water; In 1,4-dioxane; pyridine;

Reference yield:

acetic anhydride (108-24-7) + polyschistine D → 3,15-diacetylbenzoylaconine (119347-27-2)

Guidance literature:

In pyridine; Ambient temperature;

Reference yield:

acetic anhydride (108-24-7) + benzoylaconine → 15-acetylbenzoylaconine + 3,15-diacetylbenzoylaconine (119347-27-2)

Guidance literature:

for 6h; Ambient temperature;

upstream raw materials:

acetic anhydride

monoacetylaconitine

Refernces