Carbamic acid, [(1E)-2-phenylethenyl]-, 1,1-dimethylethyl ester (9CI)

Base Information

Chemical Name:Carbamic acid, [(1E)-2-phenylethenyl]-, 1,1-dimethylethyl ester (9CI)
CAS No.:648928-83-0
Molecular Formula:C13H17NO2
Molecular Weight:219.28000
Hs Code.:
Mol file:648928-83-0.mol

Synonyms:((E)-Styryl)-carbamic acid tert-butyl ester;tert-butyl (E)-styrylcarbamate;tert-butyl styrylcarbamate;

Suppliers and Price of Carbamic acid, [(1E)-2-phenylethenyl]-, 1,1-dimethylethyl ester (9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Carbamic acid, [(1E)-2-phenylethenyl]-, 1,1-dimethylethyl ester (9CI)

Chemical Property:

Melting Point:117 - 119 °C
PSA：38.33000
LogP:3.57290

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

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Technology Process of Carbamic acid, [(1E)-2-phenylethenyl]-, 1,1-dimethylethyl ester (9CI)

There total 10 articles about Carbamic acid, [(1E)-2-phenylethenyl]-, 1,1-dimethylethyl ester (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 648928-83-0
tert-butyl (E)-styrylcarbamate

Guidance literature:: With 2,4,6-trimethyl-pyridine; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; palladium dichloride; CyJohnPhos; In N,N-dimethyl acetamide; at 20 ℃; for 15h; Schlenk technique; Inert atmosphere; Irradiation;

Reference yield: 78.0%

: S-phenyl (2S)-2-[(tert-butoxycarbonyl)amino]-3-phenylpropanethioate

: 1359015-26-1
(9H-fluoren-9-yl)methyl styrylcarbamate

: 648928-83-0
tert-butyl (E)-styrylcarbamate

Guidance literature:: S-phenyl (2S)-2-[(tert-butoxycarbonyl)amino]-3-phenylpropanethioate; With copper(I) 2-hydroxy-3-methylbenzoate; palladium diacetate; triethyl phosphite; In 1,4-dioxane; at 50 ℃; for 1h; Inert atmosphere;

With palladium diacetate; triethyl phosphite; In 1,4-dioxane; at 50 ℃; for 2h; optical yield given as %de; Inert atmosphere;
DOI:10.1021/ol203399x

Reference yield: 70.0%

: S-pyridin-4-yl 2-((tert-butoxycarbonyl)amino)-3-phenylpropanethioate

: 1359015-27-2
(Z)-tert-butyl styrylcarbamate

: 648928-83-0
tert-butyl (E)-styrylcarbamate

Guidance literature:: With bis(η3-allyl-μ-chloropalladium(II)); N-ethyl-N,N-diisopropylamine; catacxium A; In 1,4-dioxane; at 105 ℃; for 18h;
DOI:10.1021/ol101620r