10H-Indolizino[1',8':2,3,4]cyclopenta[1,2-c]quinolin-6(5H)-one,7a-ethenyl-6a,7,7a,11a,12,13-hexahydro-, (6aR,7aS,11aS,13aR)- (9CI)

Base Information

Chemical Name:10H-Indolizino[1',8':2,3,4]cyclopenta[1,2-c]quinolin-6(5H)-one,7a-ethenyl-6a,7,7a,11a,12,13-hexahydro-, (6aR,7aS,11aS,13aR)- (9CI)
CAS No.:24314-58-7
Molecular Formula:C₁₉H₂₀N₂O
Molecular Weight:292.381
Hs Code.:

Synonyms:3-Epimeloscine(8CI); Meloscine, (3a)-; 10H-Indolizino[1',8':2,3,4]cyclopenta[1,2-c]quinolin-6(5H)-one,7a-ethenyl-6a,7,7a,11a,12,13-hexahydro-, [6aR-(6aa,7aa,11aa,13aR*)]-; Epimeloscine

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Chemical Property of 10H-Indolizino[1',8':2,3,4]cyclopenta[1,2-c]quinolin-6(5H)-one,7a-ethenyl-6a,7,7a,11a,12,13-hexahydro-, (6aR,7aS,11aS,13aR)- (9CI)

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MSDS Files:: SDS file from LookChem

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Technology Process of 10H-Indolizino[1',8':2,3,4]cyclopenta[1,2-c]quinolin-6(5H)-one,7a-ethenyl-6a,7,7a,11a,12,13-hexahydro-, (6aR,7aS,11aS,13aR)- (9CI)

There total 116 articles about 10H-Indolizino[1',8':2,3,4]cyclopenta[1,2-c]quinolin-6(5H)-one,7a-ethenyl-6a,7,7a,11a,12,13-hexahydro-, (6aR,7aS,11aS,13aR)- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: rac-(2aR,8bS,11aR)-11-allyl-1,1-divinyl-1,2,2a,3,4,9,10,11a-octahydro-11H-pyrrolo[3',2':2,3]cyclopenta[1,2-c]quinolin-3-one

: 24314-51-0,24314-58-7,119146-60-0,119146-61-1
(+/-)-meloscine

Guidance literature:: With Hoveyda-Grubbs catalyst second generation; In toluene; at 60 ℃; for 12h; Inert atmosphere;
DOI:10.1021/ol200311y

Reference yield: 89.0%

: (3aS*,5aR*,11bR*)-3-allyl-4,4-divinyl-2,3,3a,4,5,5a-hexahydro-1H-pyrrolo[3'',2'':2,3]cyclopenta[1,2-c]quinoline-6(7H)-one

: 24314-51-0,24314-58-7,119146-60-0,119146-61-1
(+/-)-16-epimeloscine

Guidance literature:: With Hoveyda-Grubbs catalyst second generation; In toluene; at 60 ℃; for 5h; Inert atmosphere;
DOI:10.1021/ja2042854

Reference yield: 86.0%

: 119146-71-3,131685-35-3
(6aβ,7aα,11aα,13aR^*)-7a-<2-<(o-nitrophenyl)seleno>ethyl>-6a,7,7a,11a,12,13-hexahydro-10H-indolizino<1',8':2,3,4>cyclopenta<1,2-c>quinolin-6(5H)-one

: 24314-51-0,24314-58-7,119146-60-0,119146-61-1
(+/-)-meloscine

Guidance literature:: (6aβ,7aα,11aα,13aR^*)-7a-<2-<(o-nitrophenyl)seleno>ethyl>-6a,7,7a,11a,12,13-hexahydro-10H-indolizino<1',8':2,3,4>cyclopenta<1,2-c>quinolin-6(5H)-one; With trifluoroacetic acid; In dichloromethane;

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at -78 ℃; for 1.5h;

With dimethylsulfide; triethylamine; In dichloromethane; at -78 - 20 ℃;
DOI:10.1002/chem.200802383