2H-Pyrrol-2-one,4-ethoxy-1,5-dihydro-3-(1-methoxyethenyl)-1-methyl-(9CI)

Base Information

Chemical Name:2H-Pyrrol-2-one,4-ethoxy-1,5-dihydro-3-(1-methoxyethenyl)-1-methyl-(9CI)
CAS No.:651322-77-9
Molecular Formula:C10H15NO3
Molecular Weight:197.23100
Hs Code.:
Mol file:651322-77-9.mol

Synonyms:2H-Pyrrol-2-one,4-ethoxy-1,5-dihydro-3-(1-methoxyethenyl)-1-methyl;

Suppliers and Price of 2H-Pyrrol-2-one,4-ethoxy-1,5-dihydro-3-(1-methoxyethenyl)-1-methyl-(9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

AccelPharmtech
4-ethoxy-1,5-dihydro-3-(1-methoxyethenyl)-1-methyl-2H-Pyrrol-2-one 97.00%
25G
$ 11400.00

AccelPharmtech
4-ethoxy-1,5-dihydro-3-(1-methoxyethenyl)-1-methyl-2H-Pyrrol-2-one 97.00%
1G
$ 3510.00

Total 1 raw suppliers

Chemical Property of 2H-Pyrrol-2-one,4-ethoxy-1,5-dihydro-3-(1-methoxyethenyl)-1-methyl-(9CI)

Chemical Property:

PSA：38.77000
LogP:0.84700

Purity/Quality:: 4-ethoxy-1,5-dihydro-3-(1-methoxyethenyl)-1-methyl-2H-Pyrrol-2-one 97.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2H-Pyrrol-2-one,4-ethoxy-1,5-dihydro-3-(1-methoxyethenyl)-1-methyl-(9CI)

There total 2 articles about 2H-Pyrrol-2-one,4-ethoxy-1,5-dihydro-3-(1-methoxyethenyl)-1-methyl-(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 81177-90-4
tributyl (α-methoxyethylene)tin

: 4-ethoxy-3-iodo-1-methyl-1,5-dihydro-pyrrol-2-one

: 651322-77-9
4-ethoxy-3-(1-methoxy-vinyl)-1-methyl-1,5-dihydro-pyrrol-2-one

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; In toluene; Heating;
DOI:10.1002/anie.200352591

Reference yield:

: 90968-34-6
1-Methyl-4-ethoxy-Δ³-pyrrolin-2-one

: 651322-77-9
4-ethoxy-3-(1-methoxy-vinyl)-1-methyl-1,5-dihydro-pyrrol-2-one

Guidance literature:: Multi-step reaction with 2 steps

1: 51 percent / I₂; bis(trifluoroacetoxy)iodobenzene; pyridine

2: 83 percent / [PdCl₂(PPh₃)2] / toluene / Heating

With pyridine; bis-triphenylphosphine-palladium(II) chloride; iodine; bis-[(trifluoroacetoxy)iodo]benzene; In toluene; 2: Stille reaction;
DOI:10.1002/anie.200352591