13-oxotridecanoic Acid

Base Information

Chemical Name:13-oxotridecanoic Acid
CAS No.:65157-88-2
Molecular Formula:C13H24O3
Molecular Weight:228.332
Hs Code.:
DSSTox Substance ID:DTXSID40443770
Nikkaji Number:J3.272.780H
Wikidata:Q82261716

Synonyms:13-oxotridecanoic Acid;Tridecanoic acid, 13-oxo-;brassylaldehydic acid;65157-88-2;SCHEMBL3513678;DTXSID40443770

Suppliers and Price of 13-oxotridecanoic Acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of 13-oxotridecanoic Acid

Chemical Property:

XLogP3:2.9
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:12
Exact Mass:228.17254462
Heavy Atom Count:16
Complexity:178

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C(CCCCCC=O)CCCCCC(=O)O

Technology Process of 13-oxotridecanoic Acid

There total 3 articles about 13-oxotridecanoic Acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.5%

: 616-01-3
13,14-dihydroxy-behenic acid

: 124-19-6
nonan-1-al

: 65157-88-2
13-oxotridecanoic acid

Guidance literature:: With sodium periodate; phosphoric acid; sodium carbonate;

Reference yield:

: 112-86-7
cis-13-docosenoic acid

: 124-19-6
nonan-1-al

: 65157-88-2
13-oxotridecanoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: [((S,S)-N,N′-bis(2-pyridylmethyl)-(S,S)-2,2′-bipyrrolidine)Fe^II(OTf)₂]; dihydrogen peroxide / acetic acid; acetonitrile / 24 h / 0 °C

2: sulfuric acid / acetic acid; acetonitrile; water / 24 h / 20 °C

3: sodium periodate; sodium hydrogencarbonate / acetic acid; acetonitrile; water / 24 h / 20 °C

With sodium periodate; sulfuric acid; [((S,S)-N,N′-bis(2-pyridylmethyl)-(S,S)-2,2′-bipyrrolidine)Fe^II(OTf)₂]; dihydrogen peroxide; sodium hydrogencarbonate; In water; acetic acid; acetonitrile;
DOI:10.1002/chem.201301371

Reference yield:

: 28590-30-9
12-(3-octyl-oxiranyl)-dodecanoic acid

: 124-19-6
nonan-1-al

: 65157-88-2
13-oxotridecanoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: sulfuric acid / acetic acid; acetonitrile; water / 24 h / 20 °C

2: sodium periodate; sodium hydrogencarbonate / acetic acid; acetonitrile; water / 24 h / 20 °C

With sodium periodate; sulfuric acid; sodium hydrogencarbonate; In water; acetic acid; acetonitrile;
DOI:10.1002/chem.201301371