Triacontanamide, N-[(1S,2R,3E,5R)-2,5-bis[[(1,1-dimethylethyl)dimethylsilyl]oxy]-1-[[[(1,1- dimethylethyl)dimethylsilyl]oxy]methyl]-3-heptadecenyl]-30-[[(1,1-dimeth ylethyl)diphenylsilyl]oxy]-

Base Information

Chemical Name:Triacontanamide, N-[(1S,2R,3E,5R)-2,5-bis[[(1,1-dimethylethyl)dimethylsilyl]oxy]-1-[[[(1,1- dimethylethyl)dimethylsilyl]oxy]methyl]-3-heptadecenyl]-30-[[(1,1-dimeth ylethyl)diphenylsilyl]oxy]-
CAS No.:651718-25-1
Molecular Formula:C82H155NO5Si4
Molecular Weight:1347.48
Hs Code.:

Triacontanamide,
N-[(1S,2R,3E,5R)-2,5-bis[[(1,1-dimethylethyl)dimethylsilyl]oxy]-1-[[[(1,1-
dimethylethyl)dimethylsilyl]oxy]methyl]-3-heptadecenyl]-30-[[(1,1-dimeth
ylethyl)diphenylsilyl]oxy]-

Synonyms:

Suppliers and Price of Triacontanamide, N-[(1S,2R,3E,5R)-2,5-bis[[(1,1-dimethylethyl)dimethylsilyl]oxy]-1-[[[(1,1- dimethylethyl)dimethylsilyl]oxy]methyl]-3-heptadecenyl]-30-[[(1,1-dimeth ylethyl)diphenylsilyl]oxy]-

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Triacontanamide, N-[(1S,2R,3E,5R)-2,5-bis[[(1,1-dimethylethyl)dimethylsilyl]oxy]-1-[[[(1,1- dimethylethyl)dimethylsilyl]oxy]methyl]-3-heptadecenyl]-30-[[(1,1-dimeth ylethyl)diphenylsilyl]oxy]-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Triacontanamide, N-[(1S,2R,3E,5R)-2,5-bis[[(1,1-dimethylethyl)dimethylsilyl]oxy]-1-[[[(1,1- dimethylethyl)dimethylsilyl]oxy]methyl]-3-heptadecenyl]-30-[[(1,1-dimeth ylethyl)diphenylsilyl]oxy]-

There total 4 articles about Triacontanamide, N-[(1S,2R,3E,5R)-2,5-bis[[(1,1-dimethylethyl)dimethylsilyl]oxy]-1-[[[(1,1- dimethylethyl)dimethylsilyl]oxy]methyl]-3-heptadecenyl]-30-[[(1,1-dimeth ylethyl)diphenylsilyl]oxy]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 132910-93-1
30-(tert-Butyldiphenylsilyloxy)triacontanoic acid

: 651718-24-0
(2S,3R,4E,6R)-2-amino-1,3,6-tris(tert-butyldimethylsilyloxy)-4-octadecene

: 651718-25-1
(2S,3R,4E,6R)-1,3,6-tris(tert-butyldimethylsilyloxy)-2-[30'-(tert-butyldiphenylsilyloxy)triacontanoylamino]-4-octadecene

Guidance literature:: With benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; In dichloromethane;
DOI:10.1016/j.tetlet.2003.10.025

Reference yield:

: 69739-34-0
t-butyldimethylsiyl triflate

: 651718-25-1
(2S,3R,4E,6R)-1,3,6-tris(tert-butyldimethylsilyloxy)-2-[30'-(tert-butyldiphenylsilyloxy)triacontanoylamino]-4-octadecene

Guidance literature:: Multi-step reaction with 2 steps

1: 420 mg / 2,6-lutidine / CH₂Cl₂ / 1 h / 20 °C

2: 72 percent / EDC; HOBt / CH₂Cl₂ / 12 h / 20 °C

With 2,6-dimethylpyridine; benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; In dichloromethane;
DOI:10.1002/ejoc.200500357

Reference yield:

: (2S,4E,6R)-6-hydroxy-4-sphingenine

: 651718-25-1
(2S,3R,4E,6R)-1,3,6-tris(tert-butyldimethylsilyloxy)-2-[30'-(tert-butyldiphenylsilyloxy)triacontanoylamino]-4-octadecene

Guidance literature:: Multi-step reaction with 2 steps

1: 420 mg / 2,6-lutidine / CH₂Cl₂ / 1 h / 20 °C

2: 72 percent / EDC; HOBt / CH₂Cl₂ / 12 h / 20 °C

With 2,6-dimethylpyridine; benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; In dichloromethane;
DOI:10.1002/ejoc.200500357