Benzoic acid, 3-[[6-(difluoromethoxy)-2-[[(3,4-dimethoxy-2-pyridinyl)methyl]sulfinyl]-1H -benzimidazol-1-yl]sulfonyl]-4-methyl-, 2-[(4-methylphenyl)sulfonyl]ethyl ester

Base Information

• Chemical Name: Benzoic acid, 3-[[6-(difluoromethoxy)-2-[[(3,4-dimethoxy-2-pyridinyl)methyl]sulfinyl]-1H -benzimidazol-1-yl]sulfonyl]-4-methyl-, 2-[(4-methylphenyl)sulfonyl]ethyl ester
• CAS No.: 651728-93-7
• Molecular Formula: C33H31F2N3O10S3
• Molecular Weight: 763.818

Synonyms:

Chemical Property of Benzoic acid, 3-[[6-(difluoromethoxy)-2-[[(3,4-dimethoxy-2-pyridinyl)methyl]sulfinyl]-1H -benzimidazol-1-yl]sulfonyl]-4-methyl-, 2-[(4-methylphenyl)sulfonyl]ethyl ester

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SDS file from LookChem

Useful:

Technology Process of Benzoic acid, 3-[[6-(difluoromethoxy)-2-[[(3,4-dimethoxy-2-pyridinyl)methyl]sulfinyl]-1H -benzimidazol-1-yl]sulfonyl]-4-methyl-, 2-[(4-methylphenyl)sulfonyl]ethyl ester

There total 1 articles about Benzoic acid, 3-[[6-(difluoromethoxy)-2-[[(3,4-dimethoxy-2-pyridinyl)methyl]sulfinyl]-1H -benzimidazol-1-yl]sulfonyl]-4-methyl-, 2-[(4-methylphenyl)sulfonyl]ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(R)-2-[[[3-methyl-4-(2,2,2-trifluoroethoxy)-2-pyridyl]methyl]sulfinyl]-1H-benzimidazole sodium salt + 3-chlorosulfonyl-4-methylbenzoic acid 2-(p-tolylsulfonyl)ethyl ester (651728-83-5) → 3-[5-difluoromethoxy-2-{(3,4-dimethoxy-pyridin-2-yl)-methanesulfinyl}-benzimidazole-1-sulfonyl]-4-methylbenzoic acid 2-(toluene-4-sulfonyl)ethyl ester + 3-[6-difluoromethoxy-2-{(3,4-dimethoxy-pyridin-2-yl)-methanesulfinyl}-benzimidazole-1-sulfonyl]-4-methylbenzoic acid 2-(toluene-4-sulfonyl)ethyl ester (651728-93-7)

Guidance literature:

With sodium hydrogencarbonate; triethylamine; In dichloromethane; at 20 ℃; for 2h;

Reference yield:

3-[5-difluoromethoxy-2-{(3,4-dimethoxy-pyridin-2-yl)-methanesulfinyl}-benzimidazole-1-sulfonyl]-4-methylbenzoic acid 2-(toluene-4-sulfonyl)ethyl ester + 3-[6-difluoromethoxy-2-{(3,4-dimethoxy-pyridin-2-yl)-methanesulfinyl}-benzimidazole-1-sulfonyl]-4-methylbenzoic acid 2-(toluene-4-sulfonyl)ethyl ester (651728-93-7) → 3-[5-difluoromethoxy-2-{(3,4-dimethoxy-pyridin-2-yl)-methanesulfinyl}-benzimidazole-1-sulfonyl]-4-methylbenzoic acid sodium salt + 3-[6-difluoromethoxy-2-{(3,4-dimethoxy-pyridin-2-yl)-methanesulfinyl}-benzimidazole-1-sulfonyl]-4-methylbenzoic acid sodium salt (651728-95-9)

Guidance literature:

With sodium hydrogencarbonate; In water; acetonitrile; at 65 ℃; for 2h;

upstream raw materials:

3-chlorosulfonyl-4-methylbenzoic acid 2-(p-tolylsulfonyl)ethyl ester

Downstream raw materials:

3-[6-difluoromethoxy-2-{(3,4-dimethoxy-pyridin-2-yl)-methanesulfinyl}-benzimidazole-1-sulfonyl]-4-methylbenzoic acid sodium salt

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