7-[(2-bromoacetyl)amino]-N-phenylheptanamide

Base Information

Chemical Name:7-[(2-bromoacetyl)amino]-N-phenylheptanamide
CAS No.:651767-98-5
Molecular Formula:C₁₅H₂₁BrN₂O₂
Molecular Weight:341.248
Hs Code.:
DSSTox Substance ID:DTXSID60437313
Nikkaji Number:J2.037.867K
Wikidata:Q82252795
ChEMBL ID:CHEMBL114237

Synonyms:7-[(2-bromoacetyl)amino]-N-phenylheptanamide;651767-98-5;CHEMBL114237;DTXSID60437313;BDBM50222441;N-Phenyl-7-(bromoacetylamino)heptanamide

Suppliers and Price of 7-[(2-bromoacetyl)amino]-N-phenylheptanamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 7-[(2-bromoacetyl)amino]-N-phenylheptanamide

Chemical Property:

XLogP3:2.8
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:9
Exact Mass:340.07864
Heavy Atom Count:20
Complexity:292

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)NC(=O)CCCCCCNC(=O)CBr

Technology Process of 7-[(2-bromoacetyl)amino]-N-phenylheptanamide

There total 7 articles about 7-[(2-bromoacetyl)amino]-N-phenylheptanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 505-48-6
octane-1,8-dioic acid

: 651767-98-5
7-(2-bromo-acetylamino)-heptanoic acid phenylamide

Guidance literature:: Multi-step reaction with 5 steps

1: 180 °C

2: diphenylphosphoryl azide; Et₃N / benzene / Heating

3: Heating

4: H₂ / Pd-C / methanol / 20 °C

5: Et₃N / CH₂Cl₂ / 20 °C

With diphenylphosphoranyl azide; hydrogen; triethylamine; palladium on activated charcoal; In methanol; dichloromethane; benzene; 2: Curtius rearrangement;
DOI:10.1016/j.bmcl.2004.10.074

Reference yield:

: 149648-52-2
suberanilic acid

: 651767-98-5
7-(2-bromo-acetylamino)-heptanoic acid phenylamide

Guidance literature:: Multi-step reaction with 4 steps

1: diphenylphosphoryl azide; Et₃N / benzene / Heating

2: Heating

3: H₂ / Pd-C / methanol / 20 °C

4: Et₃N / CH₂Cl₂ / 20 °C

With diphenylphosphoranyl azide; hydrogen; triethylamine; palladium on activated charcoal; In methanol; dichloromethane; benzene; 1: Curtius rearrangement;
DOI:10.1016/j.bmcl.2004.10.074

Reference yield:

: 7-isocyanato-heptanoic acid phenylamide

: 651767-98-5
7-(2-bromo-acetylamino)-heptanoic acid phenylamide

Guidance literature:: Multi-step reaction with 3 steps

1: Heating

2: H₂ / Pd-C / methanol / 20 °C

3: Et₃N / CH₂Cl₂ / 20 °C

With hydrogen; triethylamine; palladium on activated charcoal; In methanol; dichloromethane;
DOI:10.1016/j.bmcl.2004.10.074