2,2'-anhydro-1-(beta-D-arabinofuranosyl)orotic acid ethyl ester

Base Information

• Chemical Name: 2,2'-anhydro-1-(beta-D-arabinofuranosyl)orotic acid ethyl ester
• CAS No.: 33780-80-2
• Molecular Formula: C₁₂H₁₄N₂O₇
• Molecular Weight: 298.252
• Mol file: 33780-80-2.mol

Synonyms:2,2’-anhydro-1-(beta-D-arabinofuranosyl)orotic acid ethyl ester

Chemical Property of 2,2'-anhydro-1-(beta-D-arabinofuranosyl)orotic acid ethyl ester

Chemical Property:

• Boiling Point: 503.8°Cat760mmHg
• Flash Point: 258.5°C
• PSA: 120.11000
• Density: 1.82g/cm³
• LogP: -1.56840

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2,2'-anhydro-1-(beta-D-arabinofuranosyl)orotic acid ethyl ester

There total 1 articles about 2,2'-anhydro-1-(beta-D-arabinofuranosyl)orotic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-amino-β-D-arabinofurano[1',2':4,5]-oxazoline (27963-98-0) + acetylenedicarboxylic acid diethyl ester (762-21-0) → 2,2'-anhydro-1-(β-D-arabinofuranosyl) orotic acid ethyl ester (33780-80-2)

Guidance literature:

With N,N-dimethyl acetamide;

DOI:10.1021/jo00974a027

Reference yield: 78.1%

2,2'-anhydro-1-(β-D-arabinofuranosyl) orotic acid ethyl ester (33780-80-2) → 2,2'-anhydro-1-(β-D-arabinofuranosyl) orotic acid hydrazide (76580-72-8)

Guidance literature:

With hydrazine hydrate; In ethanol; for 2h; Ambient temperature;

Reference yield:

2,2'-anhydro-1-(β-D-arabinofuranosyl) orotic acid ethyl ester (33780-80-2) → (3aS)-3c-hydroxy-2t-hydroxymethyl-6-oxo-(3ar,9ac)-2,3,3a,9a-tetrahydro-6H-furo[2',3':4,5]oxazolo[3,2-a]pyrimidine-8-carboxylic acid (33886-20-3)

Guidance literature:

With potassium hydroxide; for 0.0833333h;

DOI:10.1021/jo00974a027

upstream raw materials:

2-amino-β-D-arabinofurano[1',2':4,5]-oxazoline

acetylenedicarboxylic acid diethyl ester

Downstream raw materials:

(3aS)-3c-hydroxy-2t-hydroxymethyl-6-oxo-(3ar,9ac)-2,3,3a,9a-tetrahydro-6H-furo[2',3':4,5]oxazolo[3,2-a]pyrimidine-8-carboxylic acid

2,2'-anhydro-1-(β-D-arabinofuranosyl) orotic acid hydrazide

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