1,3-Benzenedicarboxaldehyde, 2-(2-naphthalenyl)-

Base Information

Chemical Name:1,3-Benzenedicarboxaldehyde, 2-(2-naphthalenyl)-
CAS No.:652976-99-3
Molecular Formula:C18H12O2
Molecular Weight:260.292
Hs Code.:
DSSTox Substance ID:DTXSID40465174
Nikkaji Number:J2.603.254G

Synonyms:652976-99-3;1,3-Benzenedicarboxaldehyde, 2-(2-naphthalenyl)-;2-naphthalen-2-ylbenzene-1,3-dicarbaldehyde;DTXSID40465174

Suppliers and Price of 1,3-Benzenedicarboxaldehyde, 2-(2-naphthalenyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of 1,3-Benzenedicarboxaldehyde, 2-(2-naphthalenyl)-

Chemical Property:

XLogP3:3.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:260.083729621
Heavy Atom Count:20
Complexity:335

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C2C=C(C=CC2=C1)C3=C(C=CC=C3C=O)C=O

Technology Process of 1,3-Benzenedicarboxaldehyde, 2-(2-naphthalenyl)-

There total 3 articles about 1,3-Benzenedicarboxaldehyde, 2-(2-naphthalenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 32316-92-0
naphthalene-2-boronic acid

: 79839-49-9
2-bromoisophthalaldehyde

: 652976-99-3
2-(naphthalen-2-yl)benzene-1,3-dicarbaldehyde

Guidance literature:: With sodium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,2-dimethoxyethane; ethanol; Heating;
DOI:10.1021/jo030313n

Reference yield:

: 25006-88-6
2-bromo-1,3-bis(bromomethyl)benzene

: 652976-99-3
2-(naphthalen-2-yl)benzene-1,3-dicarbaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / Na₂CO₃ / Pd(PPh₃)4 / 1,2-dimethoxy-ethane; ethanol / Heating

With sodium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,2-dimethoxyethane; ethanol; 2: Suzuki coupling;
DOI:10.1021/jo030313n

Reference yield:

: 576-22-7
2-Bromo-m-xylene

: 652976-99-3
2-(naphthalen-2-yl)benzene-1,3-dicarbaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1: NBS

2: 70 percent / Na₂CO₃ / Pd(PPh₃)4 / 1,2-dimethoxy-ethane; ethanol / Heating

With N-Bromosuccinimide; sodium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,2-dimethoxyethane; ethanol; 3: Suzuki coupling;
DOI:10.1021/jo030313n