Methanesulfinic acid, trifluoro-, 4-fluorophenyl ester

Base Information

• Chemical Name: Methanesulfinic acid, trifluoro-, 4-fluorophenyl ester
• CAS No.: 655226-88-3
• Molecular Formula: C₇H₄F₄O₂S
• Molecular Weight: 228.167
• Mol file: 655226-88-3.mol

Synonyms:

Chemical Property of Methanesulfinic acid, trifluoro-, 4-fluorophenyl ester

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of Methanesulfinic acid, trifluoro-, 4-fluorophenyl ester

There total 1 articles about Methanesulfinic acid, trifluoro-, 4-fluorophenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-Fluorophenol (371-41-5) + trifluoromethylsulfinyl chloride (20621-29-8) → 4-fluorophenyl trifluoromethanesulfinate (655226-88-3)

Guidance literature:

In ethyl acetate; at 20 ℃; for 2h;

DOI:10.1016/S0022-1139(03)00106-4

Reference yield: 2.2%

4-fluorophenyl trifluoromethanesulfinate (655226-88-3) → 5,5'-difluoro-biphenyl-2,2'-diol (388-69-2) + 2-hydroxy-5-fluorophenyl trifluoromethanesulfinate

Guidance literature:

With aluminium trichloride; air; In toluene; at 20 ℃;

DOI:10.1016/S0022-1139(03)00106-4

upstream raw materials:

4-Fluorophenol

trifluoromethylsulfinyl chloride

Downstream raw materials:

5,5'-difluoro-biphenyl-2,2'-diol

Refernces