Methanone, (3-bromophenyl)(3-methyl-1-azulenyl)-

Base Information

Chemical Name:Methanone, (3-bromophenyl)(3-methyl-1-azulenyl)-
CAS No.:655237-27-7
Molecular Formula:C18H13BrO
Molecular Weight:325.205
Hs Code.:

Synonyms:Methanone,(3-bromophenyl)(3-methyl-1-azulenyl);(3-bromophenyl)(3-methylazulen-1-yl)methanone;

Suppliers and Price of Methanone, (3-bromophenyl)(3-methyl-1-azulenyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of Methanone, (3-bromophenyl)(3-methyl-1-azulenyl)-

Chemical Property:

Boiling Point:474.3±38.0 °C(Predicted)
PSA：17.07000
Density:1.389±0.06 g/cm3(Predicted)
LogP:5.09330

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Methanone, (3-bromophenyl)(3-methyl-1-azulenyl)-

There total 1 articles about Methanone, (3-bromophenyl)(3-methyl-1-azulenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 26.0%

: 1711-09-7
3-bromobenzoyl chloride

: 769-31-3
1-methylazulene

: 655237-27-7
(3-bromophenyl)(3-methylazulen-1-yl)methanone

Guidance literature:: 1-methylazulene; With aluminum (III) chloride; In dichloromethane; at 0 ℃; for 0.25h;

3-bromobenzoyl chloride; In dichloromethane; at 0 ℃; for 1h;
DOI:10.1016/j.bmc.2013.03.067

Reference yield: 46.0%

: 655237-27-7
(3-bromophenyl)(3-methylazulen-1-yl)methanone

: 655237-28-8
1-(3-bromobenzyl)-3-methylazulene

Guidance literature:: With sodium tetrahydroborate; boron trifluoride diethyl etherate; In diethyl ether; diethylene glycol dimethyl ether; at 0 - 20 ℃; for 1h;
DOI:10.1016/j.bmc.2013.03.067

Reference yield:

: 16940-66-2
sodium tetrahydroborate

: 655237-27-7
(3-bromophenyl)(3-methylazulen-1-yl)methanone

: 655237-28-8
1-(3-bromobenzyl)-3-methylazulene

Guidance literature:: (3-bromophenyl)(3-methylazulen-1-yl)methanone; With boron trifluoride diethyl etherate; In diethyl ether; diethylene glycol dimethyl ether; at 0 ℃; for 0.333333h;

sodium tetrahydroborate; In diethyl ether; diethylene glycol dimethyl ether; at 0 - 20 ℃; for 1h;